C₅H₅ZrF₂(C₆F₅NP(C₆H₅)2NC₆F₃(N(CH₃)2)2)

Base Information

• Chemical Name: C₅H₅ZrF₂(C₆F₅NP(C₆H₅)2NC₆F₃(N(CH₃)2)2)
• CAS No.: 846607-43-0
• Molecular Formula: C₃₃H₂₇F₁₀N₄PZr
• Molecular Weight: 791.786
• Mol file: 846607-43-0.mol

Synonyms:

Chemical Property of C₅H₅ZrF₂(C₆F₅NP(C₆H₅)2NC₆F₃(N(CH₃)2)2)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₅H₅ZrF₂(C₆F₅NP(C₆H₅)2NC₆F₃(N(CH₃)2)2)

There total 1 articles about C₅H₅ZrF₂(C₆F₅NP(C₆H₅)2NC₆F₃(N(CH₃)2)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

η-5-cyclopentadienyltris(dimethylamido)zirconium + C6F5NP(C6H5)2NHC6F5 (846607-30-5) + toluene (108-88-3,15644-74-3,16713-13-6) → C5H5ZrF2(C6F5NP(C6H5)2NC6F3(N(CH3)2)2) (846607-43-0) + C5H5ZrF2(NC6F4N(CH3)2P(C6H5)2NC6F4N(CH3)2)*C6H5CH3

Guidance literature:

In toluene; (N2); dropwise addn. of a soln. of ligand in toluene to a soln. of zirconium complex in toluene at -30°C, warming to room temp., stirringfor 2 d; evapn., washing with hexane, filtration, dissolving in toluene, filtration through Celite, evapn., cooling to -30°C, sepn., cooling mother liquor to -30°C; elem. anal.;

DOI:10.1021/om0492350

upstream raw materials:

C₆F₅NP(C₆H₅)2NHC₆F₅

toluene