tricarbonyl(3-phenyl-2-[(pyridine-3-carbonyl)amino]propionic acid methyl ester)(1,10-phenanthroline)rhenium(I) hexafluorophosphate

Base Information

Chemical Name:tricarbonyl(3-phenyl-2-[(pyridine-3-carbonyl)amino]propionic acid methyl ester)(1,10-phenanthroline)rhenium(I) hexafluorophosphate
CAS No.:1312104-85-0
Molecular Formula:C₃₁H₂₄N₄O₆Re*F₆P
Molecular Weight:879.726
Hs Code.:

tricarbonyl(3-phenyl-2-[(pyridine-3-carbonyl)amino]propionic acid methyl ester)(1,10-phenanthroline)rhenium(I) hexafluorophosphate

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Chemical Property of tricarbonyl(3-phenyl-2-[(pyridine-3-carbonyl)amino]propionic acid methyl ester)(1,10-phenanthroline)rhenium(I) hexafluorophosphate

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Technology Process of tricarbonyl(3-phenyl-2-[(pyridine-3-carbonyl)amino]propionic acid methyl ester)(1,10-phenanthroline)rhenium(I) hexafluorophosphate

There total 1 articles about tricarbonyl(3-phenyl-2-[(pyridine-3-carbonyl)amino]propionic acid methyl ester)(1,10-phenanthroline)rhenium(I) hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: ammonium hexafluorophosphate

: 247040-04-6
(1,10-phenanthroline)Re(CO)3CF₃SO₃

: 879123-77-0
3-phenyl-2-[(pyridine-3-carbonyl)amino]propionic acid methyl ester

: 1312104-85-0
tricarbonyl(3-phenyl-2-[(pyridine-3-carbonyl)amino]propionic acid methyl ester)(1,10-phenanthroline)rhenium(I) hexafluorophosphate

Guidance literature:: In methanol; Re complex and ligand refluxed in MeOH for 3 h; cooled; solvent removed;dissolved in min. amt. of MeOH; satd. soln. of NH4PF6 in MeOH added; H2O added; filtered; ppt. air dried; purified by pptn. from CH2Cl2 with Et2O;
DOI:10.1021/ic200252z