Fe(CO)4CH₂CHSi(C₆H₅)2OSi(C₆H₅)2CHCH₂

Base Information

• Chemical Name: Fe(CO)4CH₂CHSi(C₆H₅)2OSi(C₆H₅)2CHCH₂
• CAS No.: 79895-20-8
• Molecular Formula: C₃₂H₂₆FeO₅Si₂
• Molecular Weight: 602.573
• Mol file: 79895-20-8.mol

Synonyms:

Chemical Property of Fe(CO)4CH₂CHSi(C₆H₅)2OSi(C₆H₅)2CHCH₂

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of Fe(CO)4CH₂CHSi(C₆H₅)2OSi(C₆H₅)2CHCH₂

There total 1 articles about Fe(CO)4CH₂CHSi(C₆H₅)2OSi(C₆H₅)2CHCH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

1,1,3,3-tetraphenyl-1,3-divinyldisiloxane + diiron nonacarbonyl (15321-51-4) → (CH2CHSi(C6H5)2)2OFe(CO)3 (79895-21-9) + Fe(CO)4CH2CHSi(C6H5)2OSi(C6H5)2CHCH2 (79895-20-8)

Guidance literature:

In hexane; inert gas, mixt. stirred for 35-40°C for 2 h; solvent and volatile products eliminated in vac., Fe2(CO)9 filtered off, sepn. by chromy., first fraction gave Fe(CO)4-complex, purification by further chromy., elem. anal., second fraction gave Fe(CO)3-complex after crystn. from pentane, elem. anal.;

DOI:10.1016/S0022-328X(00)93453-3

upstream raw materials:

diiron nonacarbonyl