naphtho[1,8-cd][1,2]thiaselenole

Base Information

• Chemical Name: naphtho[1,8-cd][1,2]thiaselenole
• CAS No.: 64869-35-8
• Molecular Formula: C10H6 S Se
• Molecular Weight: 237.184

Synonyms:

Chemical Property of naphtho[1,8-cd][1,2]thiaselenole

Chemical Property:

• Vapor Pressure: 8.74E-07mmHg at 25°C
• Boiling Point: 417.2°C at 760 mmHg
• Flash Point: 206.1°C

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of naphtho[1,8-cd][1,2]thiaselenole

There total 2 articles about naphtho[1,8-cd][1,2]thiaselenole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C10H8SSe (903571-91-5) + triiodothyronine (6893-02-3,15785-49-6,7013-53-8) → naphtho<1,8-cd>thiaselenole (64869-35-8) + L-3,3'-Diiodothyronine (70-40-6,58342-32-8,4604-41-5)

Guidance literature:

With DL-dithiothreitol; at 37 ℃; pH=7.5; regioselective reaction; aq. phosphate buffer;

DOI:10.1002/anie.201005235

Reference yield:

C10H8SSe (903571-91-5) + L-thyroxine (51-48-9,24486-40-6) → naphtho<1,8-cd>thiaselenole (64869-35-8) + L-3,3',5'-triiodothyronine (5817-39-0)

Guidance literature:

With DL-dithiothreitol; at 37 ℃; pH=7.5; regioselective reaction; aq. phosphate buffer;

DOI:10.1002/anie.201005235

Reference yield: 79.0%

naphtho<1,8-cd>thiaselenole (64869-35-8) + woollins’ reagent (122039-27-4) → C16H11PSSe2 (1245625-69-7)

Guidance literature:

In toluene; for 7h; Reflux; Inert atmosphere;

DOI:10.1039/b9nj00570f

upstream raw materials:

C₁₀H₈SSe

L-thyroxine

triiodothyronine

Downstream raw materials:

C₁₆H₁₁PSSe₂

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