(C₅(CH₃)5)2Sm(Cl)(O(CH₂CH₃)2)

Base Information

Chemical Name:(C₅(CH₃)5)2Sm(Cl)(O(CH₂CH₃)2)
CAS No.:107846-38-8
Molecular Formula:C₂₄H₄₀ClOSm
Molecular Weight:530.394
Hs Code.:

(C<sub>5</sub>(CH<sub>3</sub>)5)2Sm(Cl)(O(CH<sub>2</sub>CH<sub>3</sub>)2)

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Chemical Property of (C₅(CH₃)5)2Sm(Cl)(O(CH₂CH₃)2)

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Technology Process of (C₅(CH₃)5)2Sm(Cl)(O(CH₂CH₃)2)

There total 1 articles about (C₅(CH₃)5)2Sm(Cl)(O(CH₂CH₃)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85962-90-9
Sm(η5-pentamethylcyclopentadienyl)2*diethyl ether

: 100-44-7
benzyl chloride

: {(C5Me5)2(η1-benzyl)samarium

: 3C₅(CH₃)5^(1-)*2Sm⁽³⁺⁾*3Cl^(1-)=(C₅(CH₃)5)3Sm₂Cl₃

: 107846-38-8
(C₅(CH₃)5)2Sm(Cl)(O(CH₂CH₃)2)

Guidance literature:: In benzene-d6; byproducts: bibenzyl, C5Me5CH2Ph; PhCH2Cl was gradually added to a soln. of Sm-complex in a NMR tube (1.5 equiv totally), reaction was monitored by (1)H NMR spectroscopy; all products and by-products were identified by their (1)H NMR spectra, the absence of (C5Me5)2SmCH2Ph was proved by GLC analysis of products of MeOH quench;
DOI:10.1021/om00149a039