{Me₄P}tetraphenylborate

Base Information

Chemical Name:{Me₄P}tetraphenylborate
CAS No.:15525-14-1
Molecular Formula:C₄H₁₂P*C₂₄H₂₀B
Molecular Weight:410.347
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {Me₄P}tetraphenylborate

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Technology Process of {Me₄P}tetraphenylborate

There total 1 articles about {Me₄P}tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: {(Me3PCH2)dicarbonyl(η5-cyclopentadienyl)iron}Br

: 143-66-8
sodium tetraphenyl borate

: 594-09-2
trimethylphosphane

: {(trimethylphosphine)carbonyl(η5-cyclopentadienyl)iron}tetraphenylborate

: 15525-14-1
{Me₄P}tetraphenylborate

Guidance literature:: In acetonitrile; Mixt. of CpFe(CO)2(CH2P(CH3)3)Br and PMe3 in CH3CN is kept at room temp. in the dark for 2 d, N2, filtered to remove products of decompn., clear filtrate is evapd. in vac., resulting oil is dissolved in MeOH and added to soln. of NaBPh4 in MeOH.; Ppt. is washed with methanol, recrystd. from CH2Cl2/Et2O, methanolic filtrate and washings are concd. in vac., diluted with diethyl ether, identified by NMR and IR as (Me4P)BPh4.;
DOI:10.1016/0022-328X(89)87325-5