[Ru(Cp*)(η3-2-CH3C6H4CHCHCH2)(acetonitrile)(p-CH3C6H4SO3)](1+)

Base Information

• Chemical Name: [Ru(Cp*)(η3-2-CH3C6H4CHCHCH2)(acetonitrile)(p-CH3C6H4SO3)](1+)
• CAS No.: 1169881-96-2
• Molecular Formula: C₂₉H₃₆NO₃RuS
• Molecular Weight: 579.746
• Mol file: 1169881-96-2.mol

Synonyms:

Chemical Property of [Ru(Cp*)(η3-2-CH3C6H4CHCHCH2)(acetonitrile)(p-CH3C6H4SO3)](1+)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Ru(Cp*)(η3-2-CH3C6H4CHCHCH2)(acetonitrile)(p-CH3C6H4SO3)](1+)

There total 1 articles about [Ru(Cp*)(η3-2-CH3C6H4CHCHCH2)(acetonitrile)(p-CH3C6H4SO3)](1+) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tris(acetonitrile)pentamethylcyclopentadienylruthenium(II) hexafluorophosphate + 1-(o-tolyl)-2-propen-1-ol (39627-62-8) + p-toluenesulfonic acid monohydrate (6192-52-5) → [Ru(Cp*)(η3-2-CH3C6H4CHCHCH2)(acetonitrile)(p-CH3C6H4SO3)](1+) (1164109-11-8,1169881-96-2,1169881-98-4)

Guidance literature:

In acetonitrile; under N2; 2-CH3C6H4CHCHCH2 (0.119 mmol) was added to an CH3CN soln. of Ru-contg. compd. (0.119 mmol) and p-toluenesulfonic acid moohydrate (0.119 mmol); stirring at room temp. for 30 min; the soln. was concd. under vac.; the compd. was washed with ether and dried;

DOI:10.1021/om900168y

upstream raw materials:

1-(o-tolyl)-2-propen-1-ol

p-toluenesulfonic acid monohydrate