18,18-dioxo-2,9-diphenyl-18λ⁶-5r,13c;6c,12c-dietheno-5at,12at-[2]thiapropano-[1,2,4]triazolo[1,2-a][1,2,4]triazolo[1',2':1,2]pyridazino[4,5-d]pyridazine-1,3,8,10-tetraone

Base Information

• Chemical Name: 18,18-dioxo-2,9-diphenyl-18λ⁶-5r,13c;6c,12c-dietheno-5at,12at-[2]thiapropano-[1,2,4]triazolo[1,2-a][1,2,4]triazolo[1',2':1,2]pyridazino[4,5-d]pyridazine-1,3,8,10-tetraone
• CAS No.: 64776-58-5
• Molecular Formula: C₂₈H₂₂N₆O₆S
• Molecular Weight: 570.585

Synonyms:

Chemical Property of 18,18-dioxo-2,9-diphenyl-18λ⁶-5r,13c;6c,12c-dietheno-5at,12at-[2]thiapropano-[1,2,4]triazolo[1,2-a][1,2,4]triazolo[1',2':1,2]pyridazino[4,5-d]pyridazine-1,3,8,10-tetraone

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Technology Process of 18,18-dioxo-2,9-diphenyl-18λ⁶-5r,13c;6c,12c-dietheno-5at,12at-[2]thiapropano-[1,2,4]triazolo[1,2-a][1,2,4]triazolo[1',2':1,2]pyridazino[4,5-d]pyridazine-1,3,8,10-tetraone

There total 3 articles about 18,18-dioxo-2,9-diphenyl-18λ⁶-5r,13c;6c,12c-dietheno-5at,12at-[2]thiapropano-[1,2,4]triazolo[1,2-a][1,2,4]triazolo[1',2':1,2]pyridazino[4,5-d]pyridazine-1,3,8,10-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Phenyl-1,2,4-triazolidine-3,5-dione (4233-33-4) → 18,18-dioxo-2,9-diphenyl-18λ6-5r,13c;6c,12c-dietheno-5at,12at-[2]thiapropano-[1,2,4]triazolo[1,2-a][1,2,4]triazolo[1',2':1,2]pyridazino[4,5-d]pyridazine-1,3,8,10-tetraone (64776-58-5,64812-91-5)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂

2: CH₂Cl₂

In dichloromethane;

DOI:10.1016/0040-4020(77)80411-0

Reference yield:

12-thia-[4.4.3]propella-2,4,7,9-tetraene 12,12-dioxide (23695-63-8) → 18,18-dioxo-2,9-diphenyl-18λ6-5r,13c;6c,12c-dietheno-5at,12at-[2]thiapropano-[1,2,4]triazolo[1,2-a][1,2,4]triazolo[1',2':1,2]pyridazino[4,5-d]pyridazine-1,3,8,10-tetraone (64776-58-5,64812-91-5)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂

2: CH₂Cl₂

In dichloromethane;

DOI:10.1016/0040-4020(77)80411-0

Reference yield:

4-Phenyl-1,2,4-triazolidine-3,5-dione (4233-33-4) + 15,15-dioxo-2-phenyl-15λ6-5r,10c-etheno-5at,9at-[2]thiapropano-[1,2,4]triazolo[1,2-b]phthalazine-1,3-dione (64776-53-0,64812-90-4) → 18,18-dioxo-2,9-diphenyl-18λ6-5r,13c;6c,12c-dietheno-5at,12at-[2]thiapropano-[1,2,4]triazolo[1,2-a][1,2,4]triazolo[1',2':1,2]pyridazino[4,5-d]pyridazine-1,3,8,10-tetraone (64776-58-5,64812-91-5)

Guidance literature:

In dichloromethane;

DOI:10.1016/0040-4020(77)80411-0

upstream raw materials:

4-Phenyl-1,2,4-triazolidine-3,5-dione

15,15-dioxo-2-phenyl-15λ⁶-5r,10c-etheno-5at,9at-[2]thiapropano-[1,2,4]triazolo[1,2-b]phthalazine-1,3-dione

12-thia-[4.4.3]propella-2,4,7,9-tetraene 12,12-dioxide

Downstream raw materials:

10-oxo-3,7-diphenyl-octahydro-10λ⁴-1b,3,4a,5b,7,8a-hexaaza-1,5-cyclo-1,5-[2]thiapropano-tetracyclopenta[b,def,h,jkl]biphenylene-2,4,6,8-tetraone

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