{(4'-(p-(1-methyl-4,4'-bipyridinium-1'-yl)methylphenyl)-2,2':6',2''-terpyridine)((4'-(p-N,N-di-p-anisylamino)phenyl)-2,2':6',2''-terpyridine)ruthenium}(PF₆)4

Base Information

• Chemical Name: {(4'-(p-(1-methyl-4,4'-bipyridinium-1'-yl)methylphenyl)-2,2':6',2''-terpyridine)((4'-(p-N,N-di-p-anisylamino)phenyl)-2,2':6',2''-terpyridine)ruthenium}(PF₆)4
• CAS No.: 136247-57-9
• Molecular Formula: C₆₈H₅₅N₉O₂Ru*4F₆P
• Molecular Weight: 1711.17

Synonyms:

Chemical Property of {(4'-(p-(1-methyl-4,4'-bipyridinium-1'-yl)methylphenyl)-2,2':6',2''-terpyridine)((4'-(p-N,N-di-p-anisylamino)phenyl)-2,2':6',2''-terpyridine)ruthenium}(PF₆)4

Chemical Property:

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Technology Process of {(4'-(p-(1-methyl-4,4'-bipyridinium-1'-yl)methylphenyl)-2,2':6',2''-terpyridine)((4'-(p-N,N-di-p-anisylamino)phenyl)-2,2':6',2''-terpyridine)ruthenium}(PF₆)4

There total 1 articles about {(4'-(p-(1-methyl-4,4'-bipyridinium-1'-yl)methylphenyl)-2,2':6',2''-terpyridine)((4'-(p-N,N-di-p-anisylamino)phenyl)-2,2':6',2''-terpyridine)ruthenium}(PF₆)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

potassium hexafluorophosphate (17084-13-8) + 4'-{p-(1-methyl-4,4'-bipyridinium-1'-yl)methylphenyl}-2,2':6',2''-terpyridine dichloride (136247-32-0) + ruthenium(II) (22541-59-9) + 4-([2,2′:6′,2″-terpyridin]-4′-yl)-N,N-bis(4-methoxyphenyl)aniline, (136247-34-2) → {(4'-(p-(1-methyl-4,4'-bipyridinium-1'-yl)methylphenyl)-2,2':6',2''-terpyridine)((4'-(p-N,N-di-p-anisylamino)phenyl)-2,2':6',2''-terpyridine)ruthenium}(PF6)4 (136247-57-9)

Guidance literature:

In methanol; ethanol; addn. of "ruthenium blue" soln. in methanol to a soln. of ttp-DPAA and ttp-MV(Cl)2 in ethanol under Ar, stirring under reflux for 18 h, cooling, filtn., addn. of KPF6 in water; washing of the ppt. with water, chromy. on silica gel (MeCN-aqueous soln. of KNO3);

upstream raw materials:

potassium hexafluorophosphate

4'-{p-(1-methyl-4,4'-bipyridinium-1'-yl)methylphenyl}-2,2':6',2''-terpyridine dichloride

ruthenium(II)

4-([2,2′:6′,2″-terpyridin]-4′-yl)-N,N-bis(4-methoxyphenyl)aniline,

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