RuH(CH₃OC₆H₄NNH)(P(OC₂H₅)3)4⁽¹⁺⁾*B(C₆H₅)4^(1-)={RuH(CH₃OC₆H₄NNH)(P(OC₂H₅)3)4}B(C₆H₅)4

Base Information

• Chemical Name: RuH(CH₃OC₆H₄NNH)(P(OC₂H₅)3)4⁽¹⁺⁾*B(C₆H₅)4^(1-)={RuH(CH₃OC₆H₄NNH)(P(OC₂H₅)3)4}B(C₆H₅)4
• CAS No.: 111959-75-2
• Molecular Formula: C₂₄H₂₀B*C₃₁H₆₉N₂O₁₃P₄Ru
• Molecular Weight: 1222.09

Synonyms:

Chemical Property of RuH(CH₃OC₆H₄NNH)(P(OC₂H₅)3)4⁽¹⁺⁾*B(C₆H₅)4^(1-)={RuH(CH₃OC₆H₄NNH)(P(OC₂H₅)3)4}B(C₆H₅)4

Chemical Property:

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Technology Process of RuH(CH₃OC₆H₄NNH)(P(OC₂H₅)3)4⁽¹⁺⁾*B(C₆H₅)4^(1-)={RuH(CH₃OC₆H₄NNH)(P(OC₂H₅)3)4}B(C₆H₅)4

There total 1 articles about RuH(CH₃OC₆H₄NNH)(P(OC₂H₅)3)4⁽¹⁺⁾*B(C₆H₅)4^(1-)={RuH(CH₃OC₆H₄NNH)(P(OC₂H₅)3)4}B(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

RuH2(P(OEt)3)4 (38720-12-6) + 4-methoxybenzenediazonium tetrafluoroborate (459-64-3) + sodium tetraphenyl borate (143-66-8) → RuH(CH3OC6H4NNH)(P(OC2H5)3)4(1+)*B(C6H5)4(1-)={RuH(CH3OC6H4NNH)(P(OC2H5)3)4}B(C6H5)4 (111959-75-2)

Guidance literature:

In dichloromethane; RuH2(P(OEt)3)4 in CH2Cl2 was cooled to -80 °C, addn. of the diazonium salt (ratio 1:1), warmed to 20 °C, stirred for 2 h, removal of the solvent leaving an oil, treated with EtOH, addn. of NaBPh4, filtration, precipitate dried under vacuum; crystn. by slow cooling to -30 °C of the saturated soln. in ethanol prepared by 25 °C; elemental analysis;

Reference yield:

RuH(CH3OC6H4NNH)(P(OC2H5)3)4(1+)*B(C6H5)4(1-)={RuH(CH3OC6H4NNH)(P(OC2H5)3)4}B(C6H5)4 (111959-75-2) + 4-fluorobenzenediazonium tetrafluoroborate (459-45-0) → Ru(CH3OC6H4NNH)(FC6H4NNH)(P(OC2H5)3)4(2+)*2B(C6H5)4(1-)={Ru(CH3OC6H4NNH)(FC6H4NNH)(P(OC2H5)3)4}(B(C6H5)4)2 (111959-79-6)

Guidance literature:

In dichloromethane; excess of the diazonium salt was added at 0 ° C to the soln., stirred for 70 min., filtered, evaporation of the solvent giving an oil, titurated with ethanol, addn. of NaBPh4, pptn.; crystn. from CH2Cl2/ethanol; elemental analysis;

upstream raw materials:

RuH₂(P(OEt)3)4

4-methoxybenzenediazonium tetrafluoroborate

sodium tetraphenyl borate

Downstream raw materials:

Ru(CH₃OC₆H₄NNH)(FC₆H₄NNH)(P(OC₂H₅)3)4⁽²⁺⁾*2B(C₆H₅)4^(1-)={Ru(CH₃OC₆H₄NNH)(FC₆H₄NNH)(P(OC₂H₅)3)4}(B(C₆H₅)4)2

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