[C₅H₅(CO)2(P(C₆H₅)2CH₃)Mo(CH₂)3I]

Base Information

Chemical Name:[C₅H₅(CO)2(P(C₆H₅)2CH₃)Mo(CH₂)3I]
CAS No.:383412-52-0
Molecular Formula:C₂₃H₂₄IMoO₂P
Molecular Weight:586.261
Hs Code.:

[C<sub>5</sub>H<sub>5</sub>(CO)2(P(C<sub>6</sub>H<sub>5</sub>)2CH<sub>3</sub>)Mo(CH<sub>2</sub>)3I]

Synonyms:

Suppliers and Price of [C₅H₅(CO)2(P(C₆H₅)2CH₃)Mo(CH₂)3I]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [C₅H₅(CO)2(P(C₆H₅)2CH₃)Mo(CH₂)3I]

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [C₅H₅(CO)2(P(C₆H₅)2CH₃)Mo(CH₂)3I]

There total 2 articles about [C₅H₅(CO)2(P(C₆H₅)2CH₃)Mo(CH₂)3I] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 383412-51-9
[C₅H₅(CO)2(P(C₆H₅)2CH₃)Mo(CH₂)3Br]

: 7681-82-5,24359-64-6,41927-88-2,115813-40-6
sodium iodide

: [(C₅H₅)Mo(CO)2(P(C₆H₅)2CH₃)I]

: 198906-90-0,141343-28-4
[(η5-cyclopentadienyl)(CO)2(diphenylmethylphosphine)Mo]2

: 383412-52-0
[C₅H₅(CO)2(P(C₆H₅)2CH₃)Mo(CH₂)3I]

Guidance literature:: In acetone; byproducts: NaBr; NaI was added to soln. of Mo-complex in acetone, stirred at room temp. for 18-24 h under N2; solvent was removed under reduced pressure, extd. with hexane, filtered under N2, concd. under reduced pressure, cooled to -78°C under N2, mother liquor was concd., transferred to alumina with CH2Cl2-hexane; elem. anal.;
DOI:10.1016/S0022-328X(01)01044-0

Reference yield:

: Na[(η5-cyclopentadienyl)(CO)2(diphenylmethylphosphine)Mo]

: 627-31-6
1,3-Diiodopropane

: [(C₅H₅)Mo(CO)2(P(C₆H₅)2CH₃)I]

: 198906-90-0,141343-28-4
[(η5-cyclopentadienyl)(CO)2(diphenylmethylphosphine)Mo]2

: 383412-52-0
[C₅H₅(CO)2(P(C₆H₅)2CH₃)Mo(CH₂)3I]

Guidance literature:: In tetrahydrofuran; soln. of Mo-complex in THF was added dropwise into ligand at -25-30.degre.C, stirred for 15 min, stirred at room temp. under N2; solvent was removed under reduced pressure, extd. with hexane, filtered,concd. under reduced pressure, cooled to -78°C under N2, mother liquor was syringed off, dried under reduced pressure,;
DOI:10.1016/S0022-328X(01)01044-0