(η-cyclopentadienyl)dicarbonyl(triphenoxyphosphine sulfide)iron hexafluorophosphate

Base Information

Chemical Name:(η-cyclopentadienyl)dicarbonyl(triphenoxyphosphine sulfide)iron hexafluorophosphate
CAS No.:115565-38-3
Molecular Formula:C₂₅H₂₀FeO₅PS*F₆P
Molecular Weight:664.282
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Chemical Property of (η-cyclopentadienyl)dicarbonyl(triphenoxyphosphine sulfide)iron hexafluorophosphate

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Technology Process of (η-cyclopentadienyl)dicarbonyl(triphenoxyphosphine sulfide)iron hexafluorophosphate

There total 1 articles about (η-cyclopentadienyl)dicarbonyl(triphenoxyphosphine sulfide)iron hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [Cp(CO)2Fe(THF)]PF₆

: 597-82-0
O,O,O-triphenyl phosphorothioate

: 115565-38-3
(η-cyclopentadienyl)dicarbonyl(triphenoxyphosphine sulfide)iron hexafluorophosphate

Guidance literature:: In dichloromethane; stirring of a mixture of the THF-complex and the P-ligand in CH2Cl2 at room temp. for 36 h under N2; addn. of ether, filtn. of ppt., washing (ether), drying in vacuo, recrystn. (CH2Cl2/ether), elem. anal.;
DOI:10.1016/S0020-1693(00)81752-1