W(N₂)2(P(C₂H₅)2C₆H₅)4

Base Information

• Chemical Name: W(N₂)2(P(C₂H₅)2C₆H₅)4
• CAS No.: 103352-19-8
• Molecular Formula: C₄₀H₆₀N₄P₄W
• Molecular Weight: 904.688
• Mol file: 103352-19-8.mol

Synonyms:

Chemical Property of W(N₂)2(P(C₂H₅)2C₆H₅)4

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of W(N₂)2(P(C₂H₅)2C₆H₅)4

There total 2 articles about W(N₂)2(P(C₂H₅)2C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tungsten(VI) chloride (13283-01-7) + diethyl-phenyl-phosphine (1605-53-4) → μ-dinitrogen-bis[tris(diethylphenylphosphine)bis(dinitrogen)tungsten(0)] + W(N2)2(P(C2H5)2C6H5)4 (103352-19-8)

Guidance literature:

With Mg; N₂; In tetrahydrofuran; WCl6 reacting with Mg in tne presence of the phosphine under N2 at 20°C; identified by IR, NMR spectra and single crystal X-ray diffraction;

DOI:10.1039/c39820001291

Reference yield:

WCl4(P(C2H5)2C6H5)2 (25731-33-3) + diethyl-phenyl-phosphine (1605-53-4) → μ-dinitrogen-bis[tris(diethylphenylphosphine)bis(dinitrogen)tungsten(0)] + W(N2)2(P(C2H5)2C6H5)4 (103352-19-8)

Guidance literature:

With Mg; N₂; In tetrahydrofuran; W complex reacting with Mg in the presence of the phosphine under N2 at20°C; identified by IR, NMR spectra and single crystal X-ray diffraction;

DOI:10.1039/c39820001291

upstream raw materials:

WCl₄(P(C₂H₅)2C₆H₅)2

diethyl-phenyl-phosphine

tungsten(VI) chloride