[(1,3,5-tris[bis(1-pyrazolyl)methyl]benzene)(Re(CO)3Br)2]*(CH₃)2CO

Base Information

Chemical Name:[(1,3,5-tris[bis(1-pyrazolyl)methyl]benzene)(Re(CO)3Br)2]*(CH₃)2CO
CAS No.:876127-47-8
Molecular Formula:C₃H₆O*C₃₃H₂₄Br₂N₁₂O₆Re₂
Molecular Weight:1274.93
Hs Code.:

[(1,3,5-tris[bis(1-pyrazolyl)methyl]benzene)(Re(CO)3Br)2]*(CH<sub>3</sub>)2CO

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Chemical Property of [(1,3,5-tris[bis(1-pyrazolyl)methyl]benzene)(Re(CO)3Br)2]*(CH₃)2CO

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Technology Process of [(1,3,5-tris[bis(1-pyrazolyl)methyl]benzene)(Re(CO)3Br)2]*(CH₃)2CO

There total 1 articles about [(1,3,5-tris[bis(1-pyrazolyl)methyl]benzene)(Re(CO)3Br)2]*(CH₃)2CO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14220-21-4
rhenium(I) pentacarbonyl bromide

: 876127-53-6
1,3,5-tris[bis(1-pyrazolyl)methyl]benzene

: 876127-43-4
[(1,3,5-tris[bis(1-pyrazolyl)methyl]benzene)Re(CO)3Br]

: [(1,3,5-tris[bis(1-pyrazolyl)methyl]benzene)(Re(CO)3Br)3]

: 876127-47-8
[(1,3,5-tris[bis(1-pyrazolyl)methyl]benzene)(Re(CO)3Br)2]*(CH₃)2CO

Guidance literature:: In toluene; (N2) a suspn. of Re(CO)5Br in toluene was dissolved by heating ca. 80°C, the hot soln. was added by cannula over 15 min to a refluxing toluene-soln. of an excess pyrazolyl-compound, stirred at reflux for 5 h, stirred overnight at room temp.; ppt. was filtered, washed with diethyl ether, dried in vac., layering diethyl ether onto an acetone soln.; elem. anal.;
DOI:10.1021/om0508684