1-ferrocenyl-2-(4-triphenylphosphoniophenyl)ethene bromide

Base Information

Chemical Name:1-ferrocenyl-2-(4-triphenylphosphoniophenyl)ethene bromide
CAS No.:287410-86-0
Molecular Formula:Br*C₃₆H₃₀FeP
Molecular Weight:629.359
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-ferrocenyl-2-(4-triphenylphosphoniophenyl)ethene bromide

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Technology Process of 1-ferrocenyl-2-(4-triphenylphosphoniophenyl)ethene bromide

There total 1 articles about 1-ferrocenyl-2-(4-triphenylphosphoniophenyl)ethene bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

: 350251-26-2,140874-15-3,91864-45-8
1-ferrocenyl-2-(4-bromophenyl)ethene

: 603-35-0
triphenylphosphine

: 13462-88-9
nickel dibromide

: 287410-86-0
1-ferrocenyl-2-(4-triphenylphosphoniophenyl)ethene bromide

Guidance literature:: In benzonitrile; under N2; Fe complex heated under reflux with PPh3 and NiBr2 (molar ratio 2:3:1) in benzonitrile for 4 h; cooled; extd. with CH2Cl2 and aq. KBr; org. layers dried (MgSO4); solvent evapd. in vac.; poured into Et2O; ppt. triturated many times with Et2O; filtered; solid purified by column chromy. (CH2Cl2-MeOH);
DOI:10.1016/S0022-328X(00)00085-1