1,2-(4'-F₂(C₅Me₅)CC₆F₄)2-1,2-closo-C₂B₁₀H₁₀

Base Information

Chemical Name:1,2-(4'-F₂(C₅Me₅)CC₆F₄)2-1,2-closo-C₂B₁₀H₁₀
CAS No.:1334793-89-3
Molecular Formula:C₃₆H₄₀B₁₀F₁₂
Molecular Weight:808.804
Hs Code.:

1,2-(4'-F<sub>2</sub>(C<sub>5</sub>Me<sub>5</sub>)CC<sub>6</sub>F<sub>4</sub>)2-1,2-closo-C<sub>2</sub>B<sub>10</sub>H<sub>10</sub>

Synonyms:

Suppliers and Price of 1,2-(4'-F₂(C₅Me₅)CC₆F₄)2-1,2-closo-C₂B₁₀H₁₀

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,2-(4'-F₂(C₅Me₅)CC₆F₄)2-1,2-closo-C₂B₁₀H₁₀

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,2-(4'-F₂(C₅Me₅)CC₆F₄)2-1,2-closo-C₂B₁₀H₁₀

There total 1 articles about 1,2-(4'-F₂(C₅Me₅)CC₆F₄)2-1,2-closo-C₂B₁₀H₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 1304037-86-2
1,2-(4'-CF₃C₆F₄)2-1,2-closo-C₂B₁₀H₁₀)

: sodium pentamethylcyclopentadienide

: 7646-79-9,14543-09-0,16413-89-1
cobalt(II) chloride

: 1-(4'-F₃CC₆F₄)-2,8-Cp*2-12-THF-2,8,1-closo-Co₂CB₉H₈

: 1,12-(4'-CF₃C₆F₄)2-4-C₅Me₅-4,1,12-closo-CoC₂B₁₀H₁₀

: 1334793-89-3
1,2-(4'-F₂(C₅Me₅)CC₆F₄)2-1,2-closo-C₂B₁₀H₁₀

Guidance literature:: With sodium naphthalenide; air; In tetrahydrofuran; react. a soln. of boron compd. in THF with sodium naphthalenide in THF, addn. of Cp*Na in THF, then CoCl2, stirring at room temp. for 18 h, addn. of air for 30 min; evapn. in vac., washing with petroleum ether, column chromy. (silica, CH2Cl2/petroleum ether 1:1), preparative TLC (CH2Cl2/petroleum ether 2:3);elem. anal.;
DOI:10.1021/om200691z