[(1,2-bis(diisopropylphosphino)ethane)Rh]2(μ-H)(μ-N=CHPh)

Base Information

• Chemical Name: [(1,2-bis(diisopropylphosphino)ethane)Rh]2(μ-H)(μ-N=CHPh)
• CAS No.: 146055-34-7
• Molecular Formula: C₃₅H₇₁NP₄Rh₂
• Molecular Weight: 835.661

Synonyms:

Chemical Property of [(1,2-bis(diisopropylphosphino)ethane)Rh]2(μ-H)(μ-N=CHPh)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [(1,2-bis(diisopropylphosphino)ethane)Rh]2(μ-H)(μ-N=CHPh)

There total 1 articles about [(1,2-bis(diisopropylphosphino)ethane)Rh]2(μ-H)(μ-N=CHPh) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

[(1,2-bis(diisopropylphosphino)ethane)Rh(μ-K*(tetrahydrofuran))]2 + 13C-benzonitrile (32950-71-3) → [(1,2-bis(diisopropylphosphino)ethane)Rh]2(μ-H)(μ-N=CHPh) (146055-34-7) + K[(1,2-bis(diisopropylphosphino)ethane)Rh((13)CN)(Ph)] (1344673-65-9)

Guidance literature:

In tetrahydrofuran; byproducts: KCl; under N2; by a react. of a soln. of Rh-contg. compd. in THF with (13)CN-labeled benzonitrile (0.0444 mmol); stirring for 44 h; (31)P NMR spectra monitoring; the soln. was filtered to remove KCl; the soln. was concd. to dryness and the residue was washed with hexanes; thesolid was redissolved in THF, evapd. to dryness, and dried for 1 d by v ac.; elem. anal.;

DOI:10.1021/om200342f

upstream raw materials:

¹³C-benzonitrile

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 146055-34-7 [(1,2-bis(diisopropylphosphino)ethane)Rh]2(μ-H)(μ-N=CHPh)

Send

Send

Metric Ton KG G Pound L ML

Send

Send