debromoaplysiatoxin 20,30-diacetate

Base Information

• Chemical Name: debromoaplysiatoxin 20,30-diacetate
• CAS No.: 58077-31-9
• Molecular Formula: C₃₆H₅₂O₁₂
• Molecular Weight: 676.802
• Mol file: 58077-31-9.mol

Synonyms:

Chemical Property of debromoaplysiatoxin 20,30-diacetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of debromoaplysiatoxin 20,30-diacetate

There total 3 articles about debromoaplysiatoxin 20,30-diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetic anhydride (108-24-7) + debromo aplysiatoxin (52423-28-6) → debromoaplysiatoxin 20-acetate (90359-05-0) + debromoaplysiatoxin 20,30-diacetate (58077-31-9)

Guidance literature:

With pyridine; Ambient temperature;

DOI:10.1021/jo00187a035

Reference yield:

acetic anhydride (108-24-7) + debromo aplysiatoxin (52423-28-6) → debromoaplysiatoxin 20,30-diacetate (58077-31-9)

Guidance literature:

With pyridine; Yield given; Ambient temperature;

DOI:10.1271/bbb.62.1011

Reference yield:

acetic anhydride (108-24-7) + Acetic acid (R)-1-{(1S,3R,4S,5S,9R,13S,14R)-13-hydroxy-3-[(1S,4S)-4-(3-hydroxy-phenyl)-4-methoxy-1-methyl-butyl]-4,14,16,16-tetramethyl-7,11-dioxo-2,6,10,17-tetraoxa-tricyclo[11.3.1.11,5]octadec-9-yl}-ethyl ester → debromoaplysiatoxin 20,30-diacetate (58077-31-9)

Guidance literature:

With pyridine; for 17h; Yield given; Ambient temperature;

DOI:10.1271/bbb.62.1011

upstream raw materials:

acetic anhydride

debromo aplysiatoxin