cis-(bis{(diphenylphosphinyl)methyl}phenylphosphine oxide)(tetracarbonyl tungsten⁽⁰⁾

Base Information

• Chemical Name: cis-(bis{(diphenylphosphinyl)methyl}phenylphosphine oxide)(tetracarbonyl tungsten⁽⁰⁾
• CAS No.: 121777-59-1
• Molecular Formula: C₃₆H₂₉O₇P₃W
• Molecular Weight: 850.393
• Mol file: 121777-59-1.mol

Synonyms:

Chemical Property of cis-(bis{(diphenylphosphinyl)methyl}phenylphosphine oxide)(tetracarbonyl tungsten⁽⁰⁾

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of cis-(bis{(diphenylphosphinyl)methyl}phenylphosphine oxide)(tetracarbonyl tungsten⁽⁰⁾

There total 1 articles about cis-(bis{(diphenylphosphinyl)methyl}phenylphosphine oxide)(tetracarbonyl tungsten⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

tungsten hexacarbonyl (14040-11-0) + 1,1,3,5,5-pentaphenyl-1,3,5-triphosphapentane trioxide (21851-89-8) → cis-(bis{(diphenylphosphinyl)methyl}phenylphosphine oxide)(tetracarbonyl tungsten(0) (121777-59-1)

Guidance literature:

In xylene; Ar atmosphere, metal/ligand ratio 2:1, refluxing (40 min); filtration, washing (xylene), drying (water suction-pipe); elem. anal.;

DOI:10.1016/S0277-5387(00)83824-3

upstream raw materials:

tungsten hexacarbonyl

1,1,3,5,5-pentaphenyl-1,3,5-triphosphapentane trioxide