Diazene, (1-chlorocyclohexyl)(2,4,6-trichlorophenyl)-

Base Information

Chemical Name:Diazene, (1-chlorocyclohexyl)(2,4,6-trichlorophenyl)-
CAS No.:143643-96-3
Molecular Formula:C12H12Cl4N2
Molecular Weight:326.053
Hs Code.:
DSSTox Substance ID:DTXSID10464199

Synonyms:Diazene, (1-chlorocyclohexyl)(2,4,6-trichlorophenyl)-;143643-96-3;DTXSID10464199;1-[(1-chloro-cyclohexyl)azo]-2,4,6-trichlorobenzene

Suppliers and Price of Diazene, (1-chlorocyclohexyl)(2,4,6-trichlorophenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Diazene, (1-chlorocyclohexyl)(2,4,6-trichlorophenyl)-

Chemical Property:

XLogP3:6.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:325.972509
Heavy Atom Count:18
Complexity:293

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(CC1)(N=NC2=C(C=C(C=C2Cl)Cl)Cl)Cl

Technology Process of Diazene, (1-chlorocyclohexyl)(2,4,6-trichlorophenyl)-

There total 3 articles about Diazene, (1-chlorocyclohexyl)(2,4,6-trichlorophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 15254-11-2
1-cyclohexylidene-2-(2,4,6-trichlorophenyl)hydrazine

: 143643-96-3
1-<(1-Chlorocyclohexyl)azo>-2,4,6-trichlorobenzene

Guidance literature:: With tert-butylhypochlorite; In chloroform; at 0 ℃; for 3h;
DOI:10.1055/s-1992-26206

Reference yield:

: 5329-12-4
(2,4,6-trichlorophenyl)hydrazine

: 143643-96-3
1-<(1-Chlorocyclohexyl)azo>-2,4,6-trichlorobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / AcOH / ethanol / 5 h / Heating

2: 78 percent / t-BuOCl / CHCl₃ / 3 h / 0 °C

With tert-butylhypochlorite; acetic acid; In ethanol; chloroform;
DOI:10.1055/s-1992-26206

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 143643-96-3
1-<(1-Chlorocyclohexyl)azo>-2,4,6-trichlorobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / AcOH / ethanol / 5 h / Heating

2: 78 percent / t-BuOCl / CHCl₃ / 3 h / 0 °C

With tert-butylhypochlorite; acetic acid; In ethanol; chloroform;
DOI:10.1055/s-1992-26206