(HgBr₂(HP(C₆H₁₁)2))2

Base Information

• Chemical Name: (HgBr₂(HP(C₆H₁₁)2))2
• CAS No.: 91885-96-0
• Molecular Formula: C₂₄H₄₆Br₄Hg₂P₂
• Molecular Weight: 1117.37

Synonyms:

Chemical Property of (HgBr₂(HP(C₆H₁₁)2))2

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (HgBr₂(HP(C₆H₁₁)2))2

There total 1 articles about (HgBr₂(HP(C₆H₁₁)2))2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

mercury dibromide + dicyclohexylphosphane (829-84-5) → (HgBr2(HP(C6H11)2))2 (91885-96-0)

Guidance literature:

In dichloromethane; appropriate amts. HPcycl2 and HgBr2 in dichloromethane stirred for 15 min under N2; ethanol added;

DOI:10.1016/S0020-1693(00)83613-0

Reference yield:

(HgBr2(HP(C6H11)2))2 (91885-96-0) + tetrabutylammomium bromide (1643-19-2) → (HgBr3(HP(C6H11)2))(1-)

Guidance literature:

In dichloromethane; react. appropriate amts. Bu4NBr with (HgBr2(HPcycl2))2 in CH2Cl2 under N2 atm.; not isolated;

DOI:10.1016/S0020-1693(00)83613-0

Reference yield:

(HgBr2(HP(C6H11)2))2 (91885-96-0) + 1-(dicyclohexylphosphino)-N-phenylthioformamide (899-27-4) → HgBr2((C6H11)2PH)((C6H11)2PC(S)N(H)C6H5) (91885-84-6)

Guidance literature:

In dichloromethane; react. (HgBr2(HPcycl2))2 and (1-(dicyclohexylphosphino))-N-phenylthioformamide (1:2) in CH2Cl2 under N2;

DOI:10.1016/S0020-1693(00)83613-0

upstream raw materials:

dicyclohexylphosphane

Downstream raw materials:

HgBr₂((C₆H₁₁)2PH)((C₆H₁₁)2PC(S)N(H)C₆H₅)

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