2,2,4,4-tetraphenyl-6-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropoxy-propoxy)-ethyl]-2λ⁵,4λ⁵-[1,3,5,2,4]triazadiphosphinine

Base Information

• Chemical Name: 2,2,4,4-tetraphenyl-6-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropoxy-propoxy)-ethyl]-2λ⁵,4λ⁵-[1,3,5,2,4]triazadiphosphinine
• CAS No.: 70242-76-1
• Molecular Formula: C₃₃H₂₀F₁₇N₃O₂P₂
• Molecular Weight: 875.461

Synonyms:

Chemical Property of 2,2,4,4-tetraphenyl-6-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropoxy-propoxy)-ethyl]-2λ⁵,4λ⁵-[1,3,5,2,4]triazadiphosphinine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2,4,4-tetraphenyl-6-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropoxy-propoxy)-ethyl]-2λ⁵,4λ⁵-[1,3,5,2,4]triazadiphosphinine

There total 3 articles about 2,2,4,4-tetraphenyl-6-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropoxy-propoxy)-ethyl]-2λ⁵,4λ⁵-[1,3,5,2,4]triazadiphosphinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3,3,3-Tetrafluoro-2-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropyloxy-propoxy)-propionamidine + diphenyltrichlorophosphorane (1017-89-6) → 2,2,4,4-tetraphenyl-6-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropoxy-propoxy)-ethyl]-2λ5,4λ5-[1,3,5,2,4]triazadiphosphinine (70242-76-1) + 2,2-diphenyl-4,6-bis-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropoxy-propoxy)-ethyl]-2λ5-[1,3,5,2]triazaphosphinine (65288-70-2) + (1Z,4Z)-2,2,6,6-Tetraphenyl-4,8-bis-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropyloxy-propoxy)-ethyl]-2λ5,6λ5-[1,3,5,7,2,6]tetrazadiphosphocine

Guidance literature:

Title compound not separated from byproducts; 1.) 108 - 114 deg C, 24 h, 2.) 123 - 132 deg C, 114 h;

DOI:10.1016/S0022-1139(00)82365-9

Reference yield:

imido-tetraphenyl-diphosphinic acid trichloride + 2,3,3,3-Tetrafluoro-2-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropyloxy-propoxy)-N-[2,3,3,3-tetrafluoro-2-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropyloxy-propoxy)-1-imino-propyl]-propionamidine → 2,2,4,4-tetraphenyl-6-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropoxy-propoxy)-ethyl]-2λ5,4λ5-[1,3,5,2,4]triazadiphosphinine (70242-76-1) + 2,2-diphenyl-4,6-bis-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropoxy-propoxy)-ethyl]-2λ5-[1,3,5,2]triazaphosphinine (65288-70-2)

Guidance literature:

at 102 - 138 ℃; for 253h; Product distribution; various solvents, time and temp.;

DOI:10.1016/S0022-1139(00)82365-9

Reference yield:

→ 2,2,4,4-tetraphenyl-6-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropoxy-propoxy)-ethyl]-2λ5,4λ5-[1,3,5,2,4]triazadiphosphinine (70242-76-1)

Guidance literature:

Imido-tetraphenyl-diphosphinsaeuredichlorid, C3F7OCF(CF3)CF2OCF(CF3)C(=NH)NH2, Δ;

DOI:10.1016/S0022-1139(00)82087-4

upstream raw materials:

diphenyltrichlorophosphorane

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