2H-Azirine-2-carboxylic acid, 3-methyl-, ethyl ester

Base Information

• Chemical Name: 2H-Azirine-2-carboxylic acid, 3-methyl-, ethyl ester
• CAS No.: 14369-88-1
• Molecular Formula: C6H9NO2
• Molecular Weight: 127.143
• Mol file: 14369-88-1.mol

Synonyms:ethyl 3-methyl-2H-azirine-2-carboxylate;3-methyl-2H-azirine-2-carboxylic acid ethyl ester;3-Methyl-2-carbethoxy-2h-aziren;3-Methyl-2H-aziren-2-carbonsaeure-ethylester;

Chemical Property of 2H-Azirine-2-carboxylic acid, 3-methyl-, ethyl ester

Chemical Property:

• PSA: 38.66000
• LogP: -0.17180

Purity/Quality:

99%, ^*data from raw suppliers

Ethyl3-methyl-2H-azirine-2-carboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2H-Azirine-2-carboxylic acid, 3-methyl-, ethyl ester

There total 6 articles about 2H-Azirine-2-carboxylic acid, 3-methyl-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C13H17NO5S (604787-00-0) → (±)-ethyl 3-methyl-2H-azirine-2-carboxylate (14369-88-1)

Guidance literature:

With triethylamine; In dichloromethane; Ambient temperature;

DOI:10.1021/ja961414o

Reference yield:

ethyl 3-oxobutanate oxime (5447-76-7) → (±)-ethyl 3-methyl-2H-azirine-2-carboxylate (14369-88-1)

Guidance literature:

Multi-step reaction with 2 steps

1: Py / CH₂Cl₂

2: Et₃N / CH₂Cl₂ / Ambient temperature

With pyridine; triethylamine; In dichloromethane;

DOI:10.1021/ja961414o

Reference yield:

ethyl acetoacetate (141-97-9) → (±)-ethyl 3-methyl-2H-azirine-2-carboxylate (14369-88-1)

Guidance literature:

Multi-step reaction with 3 steps

1: NH₂OH*HCl, aq. NaOH / methanol

2: Py / CH₂Cl₂

3: Et₃N / CH₂Cl₂ / Ambient temperature

With pyridine; sodium hydroxide; hydroxylamine hydrochloride; triethylamine; In methanol; dichloromethane;

DOI:10.1021/ja961414o

upstream raw materials:

C₁₃H₁₇NO₅S

ethyl 3-oxobutanate oxime

ethyl acetoacetate

Downstream raw materials:

2'-Ethyl-4'-methyl-3'-phenyl-2,3,4,5,2',3'-hexahydro-1'H-[1,2']bipyrrolyl-5'-carboxylic acid ethyl ester

ethyl 5-ethyl-3,4-dimethylpyrrole-2-carboxylate

ethyl 3-methyl-4,5,6,7-tetrahydro-1H-indole-2-carboxylate

2-Ethoxycarbonyl-3-methyl-cycloheptenopyrrol

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