3,5-Di-t-butylbenzoyl chloride

Base Information

Chemical Name:3,5-Di-t-butylbenzoyl chloride
CAS No.:14377-33-4
Molecular Formula:C15H21ClO
Molecular Weight:252.784
Hs Code.:
DSSTox Substance ID:DTXSID30473607
Nikkaji Number:J1.340.498D
Wikidata:Q82303113

Synonyms:3,5-di-t-butylbenzoyl chloride;3,5-di-tert-butylbenzoyl chloride;14377-33-4;SCHEMBL2965925;DTXSID30473607;HZBWOZJDPPOMOM-UHFFFAOYSA-N;AKOS015958559;FT-0747638

Suppliers and Price of 3,5-Di-t-butylbenzoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3,5-Di-t-butylbenzoyl chloride

Chemical Property:

XLogP3:5.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:252.1280930
Heavy Atom Count:17
Complexity:260

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)C1=CC(=CC(=C1)C(=O)Cl)C(C)(C)C

Technology Process of 3,5-Di-t-butylbenzoyl chloride

There total 4 articles about 3,5-Di-t-butylbenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 16225-26-6
3,5-di-tert-butylbenzoic acid

: 14377-33-4
3,5-di-tert-butylbenzoyl chloride

Guidance literature:: With thionyl chloride; N,N-dimethyl-formamide; for 4h; Reflux;
DOI:10.1016/j.bmc.2016.09.046

Reference yield: 99.0%

: 14377-33-4
3,5-di-tert-butylbenzoyl chloride

Guidance literature:

Reference yield:

: 22385-77-9
1-bromo-3,5-di-tert-butylbenzene

: 14377-33-4
3,5-di-tert-butylbenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) LiBu / 1.) THF, ether, -78 deg C, 3 h, 2.) THF, -78 deg C to RT

2: SOCl₂ / Heating

With n-butyllithium; thionyl chloride;
DOI:10.1016/0022-328X(92)83302-X