2-[1-Iodo-2-[(4-methylphenyl)sulfonyl]ethyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-[1-Iodo-2-[(4-methylphenyl)sulfonyl]ethyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:143825-85-8
Molecular Formula:C₁₅H₂₂BIO₄S
Molecular Weight:436.119
Hs Code.:
DSSTox Substance ID:DTXSID501129331

Synonyms:DTXSID501129331;2-[1-Iodo-2-[(4-methylphenyl)sulfonyl]ethyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane;143825-85-8

Suppliers and Price of 2-[1-Iodo-2-[(4-methylphenyl)sulfonyl]ethyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[1-Iodo-2-[(4-methylphenyl)sulfonyl]ethyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:436.03766
Heavy Atom Count:22
Complexity:476

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:B1(OC(C(O1)(C)C)(C)C)C(CS(=O)(=O)C2=CC=C(C=C2)C)I

Technology Process of 2-[1-Iodo-2-[(4-methylphenyl)sulfonyl]ethyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 1 articles about 2-[1-Iodo-2-[(4-methylphenyl)sulfonyl]ethyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1950-78-3
p-toluenesulfonyl iodide

: 75927-49-0
pinacol vinylboronate

: 143825-85-8
CH₃C₆H₄SO₂CH₂CHIB(O₂C(CH₃)2C(CH₃)2)

Guidance literature:: In dichloromethane; (N2); paratoluenesulfonyl iodide was added to soln. of B-compound ; soln. was kept at room temp.for 12 h; solvent was removed in vac.; ppt. was recrystd.; elem. anal.;

Reference yield: 87.0%

: 143825-85-8
CH₃C₆H₄SO₂CH₂CHIB(O₂C(CH₃)2C(CH₃)2)

: 6674-22-2,83329-50-4
1,8-diazabicyclo[5.4.0]undec-7-ene

: 143825-92-7
4,4,5,5-Tetramethyl-2-[(E)-2-(toluene-4-sulfonyl)-vinyl]-[1,3,2]dioxaborolane

Guidance literature:: In dichloromethane; (N2); diazabicycloundecene (DBU) was added to B-compound at 0°C; 12 h at room temp.; solvent was removed in vac.; ether was added; ppt. was removed by filtration through a pad of silica gel; ether was removed; ppt. was recrystd. from hexane/ether (9:1); elem. anal.;