4-{1',2'-bis(diphenylphosphino)ethane}-closo-1,6-dicarba-4-palladatridecaborane

Base Information

Chemical Name:4-{1',2'-bis(diphenylphosphino)ethane}-closo-1,6-dicarba-4-palladatridecaborane
CAS No.:114935-33-0
Molecular Formula:C₂₈H₃₆B₁₀P₂Pd
Molecular Weight:649.071
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-{1',2'-bis(diphenylphosphino)ethane}-closo-1,6-dicarba-4-palladatridecaborane

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Technology Process of 4-{1',2'-bis(diphenylphosphino)ethane}-closo-1,6-dicarba-4-palladatridecaborane

There total 1 articles about 4-{1',2'-bis(diphenylphosphino)ethane}-closo-1,6-dicarba-4-palladatridecaborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 19978-61-1
(1,2-bis(diphenylphosphanyl)ethane)dichloridopalladium(II)

: 2Na⁽¹⁺⁾*(C₂B₁₀H₁₂)^(2-)=Na₂(C₂B₁₀H₁₂)

: 114935-33-0
4-{1',2'-bis(diphenylphosphino)ethane}-closo-1,6-dicarba-4-palladatridecaborane

Guidance literature:: In dichloromethane; PdCl2(dppe) was added slowly to a stirred soln. of Na2(C2B10H12) in CH2Cl2 under N2, mixt. was stirred for 0.5 h; filtered in air, (dppe)PdC2B10H12 was isolated by flash chromy. (SiO2, CH2Cl2), recrystd. from CH2Cl2; elem. anal. (0.5CH2Cl2 solvate);