tris(4-hydroxy-3,5-di-tert-butylbenzonitrile)rhodium trichloride

Base Information

• Chemical Name: tris(4-hydroxy-3,5-di-tert-butylbenzonitrile)rhodium trichloride
• CAS No.: 91320-81-9
• Molecular Formula: C₄₅H₆₃Cl₃N₃O₃Rh
• Molecular Weight: 903.278
• Mol file: 91320-81-9.mol

Synonyms:

Chemical Property of tris(4-hydroxy-3,5-di-tert-butylbenzonitrile)rhodium trichloride

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of tris(4-hydroxy-3,5-di-tert-butylbenzonitrile)rhodium trichloride

There total 1 articles about tris(4-hydroxy-3,5-di-tert-butylbenzonitrile)rhodium trichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

rhodium(III) chloride trihydrate + 2,6-di-tert-butyl-4-cyanophenol (1988-88-1) → tris(4-hydroxy-3,5-di-tert-butylbenzonitrile)rhodium trichloride (91320-81-9)

Guidance literature:

In ethanol; Ar atmosphere; addn. of RhCl3*3H2O in alcohol to soln. of ligand, boiling (2 days); cooling, concn. (evapn.), chromy. (silica gel, benzene, alcohol); elem.anal.;

DOI:10.1007/BF01141723

upstream raw materials:

2,6-di-tert-butyl-4-cyanophenol