2-phenyl-1,3,2-diaza-thiophosphoryl-[3]ferrocenophane

Base Information

Chemical Name:2-phenyl-1,3,2-diaza-thiophosphoryl-[3]ferrocenophane
CAS No.:767334-52-1
Molecular Formula:C₁₆H₁₅FeN₂PS
Molecular Weight:354.195
Hs Code.:

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Chemical Property of 2-phenyl-1,3,2-diaza-thiophosphoryl-[3]ferrocenophane

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Technology Process of 2-phenyl-1,3,2-diaza-thiophosphoryl-[3]ferrocenophane

There total 1 articles about 2-phenyl-1,3,2-diaza-thiophosphoryl-[3]ferrocenophane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1,1'-ferrocene diamine

: 7704-34-9
sulfur

: 644-97-3
Dichlorophenylphosphine

: 767334-52-1
2-phenyl-1,3,2-diaza-thiophosphoryl-[3]ferrocenophane

: 767334-54-3,767334-53-2
Fe(C₅H₄N(P(Cl)C₆H₅)P(C₆H₅)NHC₅H₄)

Guidance literature:: With Et₃N; In diethyl ether; toluene; byproducts: Et3NHCl; all manipulations in absence of air and moisture; suspn. of Fe compd. with Et3N in Et2O cooled to 0°C, soln. of P compd. in Et2O added dropwise, stirred for 2 h at 0°C, allowed to warm to room temp., stirred for 20 h; filtered, volatiles removed in vac., oily-residue dissolved in Et2O, filtered, solvent removed in vac., residue dissolved in toluene, S added, stirred for 4 h, filtered, solvent removed in vac.;
DOI:10.1016/j.inoche.2004.04.026