Co(P(CH₃)3)3(SP(C₆H₅)2C₆H₄)

Base Information

Chemical Name:Co(P(CH₃)3)3(SP(C₆H₅)2C₆H₄)
CAS No.:1017235-66-3
Molecular Formula:C₂₇H₄₁CoP₄S
Molecular Weight:580.577
Hs Code.:

Co(P(CH<sub>3</sub>)3)3(SP(C<sub>6</sub>H<sub>5</sub>)2C<sub>6</sub>H<sub>4</sub>)

Synonyms:

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Chemical Property of Co(P(CH₃)3)3(SP(C₆H₅)2C₆H₄)

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Technology Process of Co(P(CH₃)3)3(SP(C₆H₅)2C₆H₄)

There total 4 articles about Co(P(CH₃)3)3(SP(C₆H₅)2C₆H₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 210900-66-6
mer-hydrido(2-oxo-naphthalene-formyl)tris(trimethylphosphine)cobalt(III)

: 119327-17-2
(2-mercaptophenyl)diphenylphosphine

: 1017235-66-3
Co(P(CH₃)3)3(SP(C₆H₅)2C₆H₄)

: 1017235-63-0,1018071-03-8
(2-oxo-naphthalene-formyl)[(1-formyl)naphtholato(O,O)]bis(trimethylphosphine)cobalt(III)

: Co(P(CH₃)3)(SP(C₆H₅)2C₆H₄)2

Guidance literature:: In diethyl ether; equimolar Et2O soln. of organic ligand added slowly at room temp. to Co-complex in Et2O; stirred at room temp. for 18 h; volatiles evapd. under vacuum; extracted with pentane, Et2O and THF; crystallized at -27°C from pentane or THF; elem. anal.;
DOI:10.1016/j.poly.2007.11.010

Reference yield: 25.0%

: 210900-98-4
mer-hydrido-(1-carbonyl-2-oxo-1,2-diphenylethenediyl)tris(trimethylphosphane)cobalt(III)

: 119327-17-2
(2-mercaptophenyl)diphenylphosphine

: 1017235-66-3
Co(P(CH₃)3)3(SP(C₆H₅)2C₆H₄)

: (1-carbonyl-2-oxo-1,2-diphenylethenyl)[(1-formyl-2-oxo-1,2-diphenylethenyl)(O,O)]bis(trimethylphosphine)cobalt(III)

: Co(P(CH₃)3)(SP(C₆H₅)2C₆H₄)2

Guidance literature:: In diethyl ether; equimolar Et2O soln. of organic ligand added slowly at room temp. to Co-complex in Et2O; stirred at room temp. for 18 h; volatiles evapd. under vacuum; extracted with pentane, Et2O and THF; crystallized at -27°C from pentane or THF; elem. anal.;
DOI:10.1016/j.poly.2007.11.010

Reference yield: 9.0%

: 210900-91-7
mer-hydrido-(1-carbonyl-2-oxo-cyclohexenediyl)tris(trimethylphosphane)cobalt(III)

: 119327-17-2
(2-mercaptophenyl)diphenylphosphine

: 1017235-66-3
Co(P(CH₃)3)3(SP(C₆H₅)2C₆H₄)

: Co(P(CH₃)3)2(COOC₆H₈)(COOHC₆H₈)

: Co(P(CH₃)3)2(COOC₆H₈)(COOHC₆H₈)

: 1017235-59-4
trans-[(1-carbonyl-2-oxo-cyclohexenediyl)-(2-diphenylphosphanyl)thiophenyl(S,P)] bis(trimethylphosphine)cobalt(III)

: Co(P(CH₃)3)(SP(C₆H₅)2C₆H₄)2

Guidance literature:: In diethyl ether; Et2O soln. of organic ligand added slowly at -80°C to Co-complex in Et2O; stirred at ambient temp. for 18 h; volatiles evapd. under vacuum; extracted with pentane and Et2O; crystallized at -27°C from pentane or THF or Et2O; elem. anal.;
DOI:10.1016/j.poly.2007.11.010