[(4S,5S)-5-(Hydroxy-diphenyl-methyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-diphenyl-methanol; compound with 4,4a,5,6,7,8-hexahydro-3H-naphthalen-2-one

Base Information

• Chemical Name: [(4S,5S)-5-(Hydroxy-diphenyl-methyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-diphenyl-methanol; compound with 4,4a,5,6,7,8-hexahydro-3H-naphthalen-2-one
• CAS No.: 117859-41-3
• Molecular Formula: C₁₀H₁₄O*C₃₁H₃₀O₄
• Molecular Weight: 616.797

Synonyms:

Chemical Property of [(4S,5S)-5-(Hydroxy-diphenyl-methyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-diphenyl-methanol; compound with 4,4a,5,6,7,8-hexahydro-3H-naphthalen-2-one

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Technology Process of [(4S,5S)-5-(Hydroxy-diphenyl-methyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-diphenyl-methanol; compound with 4,4a,5,6,7,8-hexahydro-3H-naphthalen-2-one

There total 3 articles about [(4S,5S)-5-(Hydroxy-diphenyl-methyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-diphenyl-methanol; compound with 4,4a,5,6,7,8-hexahydro-3H-naphthalen-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4S,5S)-diethyl 2,2-dimethyl-1,3-dioxolane-4,5-dicarboxylate (73346-73-3) → [(4S,5S)-5-(Hydroxy-diphenyl-methyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-diphenyl-methanol; compound with 4,4a,5,6,7,8-hexahydro-3H-naphthalen-2-one (117859-41-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / tetrahydrofuran

2: benzene; hexane / 12 h / Ambient temperature

In tetrahydrofuran; hexane; benzene;

DOI:10.1016/S0040-4039(00)80147-1

Reference yield:

phenylmagnesium bromide → [(4S,5S)-5-(Hydroxy-diphenyl-methyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-diphenyl-methanol; compound with 4,4a,5,6,7,8-hexahydro-3H-naphthalen-2-one (117859-41-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / tetrahydrofuran

2: benzene; hexane / 12 h / Ambient temperature

In tetrahydrofuran; hexane; benzene;

DOI:10.1016/S0040-4039(00)80147-1

Reference yield:

4,4a,5,6,7,8-hexahydronaphthalen-2(3H)-one (1196-55-0) + (S,S)-taddol (93222-42-5,93379-48-7,93379-49-8,118139-82-5,126639-52-9,37031-30-4) → [(4S,5S)-5-(Hydroxy-diphenyl-methyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-diphenyl-methanol; compound with 4,4a,5,6,7,8-hexahydro-3H-naphthalen-2-one (117859-41-3)

Guidance literature:

In hexane; benzene; for 12h; Ambient temperature;

DOI:10.1016/S0040-4039(00)80147-1

upstream raw materials:

4,4a,5,6,7,8-hexahydronaphthalen-2(3H)-one

(S,S)-taddol

(4S,5S)-diethyl 2,2-dimethyl-1,3-dioxolane-4,5-dicarboxylate

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