3-(Cyclohexyloxy)-4-methoxybenzoyl chloride

Base Information

Chemical Name:3-(Cyclohexyloxy)-4-methoxybenzoyl chloride
CAS No.:144036-20-4
Molecular Formula:C14H17ClO3
Molecular Weight:268.74
Hs Code.:
DSSTox Substance ID:DTXSID401260796
Mol file:144036-20-4.mol

Synonyms:SCHEMBL7336558;DTXSID401260796;144036-20-4;3-(Cyclohexyloxy)-4-methoxybenzoyl chloride

Suppliers and Price of 3-(Cyclohexyloxy)-4-methoxybenzoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(Cyclohexyloxy)-4-methoxybenzoyl chloride

Chemical Property:

XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:268.0866221
Heavy Atom Count:18
Complexity:276

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)C(=O)Cl)OC2CCCCC2

Technology Process of 3-(Cyclohexyloxy)-4-methoxybenzoyl chloride

There total 4 articles about 3-(Cyclohexyloxy)-4-methoxybenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 144036-18-0
3-Cyclohexyloxy-4-methoxy-benzoic acid

: 144036-20-4
3-Cyclohexyloxy-4-methoxy-benzoyl chloride

Guidance literature:: With thionyl chloride; In N,N-dimethyl-formamide; toluene; for 5h; Heating;
DOI:10.1021/jm00037a021

Reference yield:

: 621-59-0
isovanillin

: 144036-20-4
3-Cyclohexyloxy-4-methoxy-benzoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃, KI / dimethylformamide / 21 h / 65 °C

2: sulfamic acid, aq. AcOH, aq. NaClO₂ / 1 h / Ambient temperature

3: SOCl₂ / toluene; dimethylformamide / 5 h / Heating

With sodium chlorite; thionyl chloride; aminosulfonic acid; potassium carbonate; acetic acid; potassium iodide; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00037a021

Reference yield:

: 108-85-0
1-bromocyclohexane

: 144036-20-4
3-Cyclohexyloxy-4-methoxy-benzoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃, KI / dimethylformamide / 21 h / 65 °C

2: sulfamic acid, aq. AcOH, aq. NaClO₂ / 1 h / Ambient temperature

3: SOCl₂ / toluene; dimethylformamide / 5 h / Heating

With sodium chlorite; thionyl chloride; aminosulfonic acid; potassium carbonate; acetic acid; potassium iodide; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00037a021