Cd⁽²⁺⁾*(C₃H₆)2(C₂H₄)2N₄H₂(CH₂C₆H₅)2*NO₃^(1-)*PF₆^(1-)=[Cd((C₃H₆)2(C₂H₄)2N₄H₂(CH₂C₆H₅)2)(NO₃)]PF₆

Base Information

• Chemical Name: Cd⁽²⁺⁾*(C₃H₆)2(C₂H₄)2N₄H₂(CH₂C₆H₅)2*NO₃^(1-)*PF₆^(1-)=[Cd((C₃H₆)2(C₂H₄)2N₄H₂(CH₂C₆H₅)2)(NO₃)]PF₆
• CAS No.: 578737-68-5
• Molecular Formula: C₂₄H₃₆N₄*Cd*F₆P*NO₃
• Molecular Weight: 699.956

Synonyms:

Chemical Property of Cd⁽²⁺⁾*(C₃H₆)2(C₂H₄)2N₄H₂(CH₂C₆H₅)2*NO₃^(1-)*PF₆^(1-)=[Cd((C₃H₆)2(C₂H₄)2N₄H₂(CH₂C₆H₅)2)(NO₃)]PF₆

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Technology Process of Cd⁽²⁺⁾*(C₃H₆)2(C₂H₄)2N₄H₂(CH₂C₆H₅)2*NO₃^(1-)*PF₆^(1-)=[Cd((C₃H₆)2(C₂H₄)2N₄H₂(CH₂C₆H₅)2)(NO₃)]PF₆

There total 1 articles about Cd⁽²⁺⁾*(C₃H₆)2(C₂H₄)2N₄H₂(CH₂C₆H₅)2*NO₃^(1-)*PF₆^(1-)=[Cd((C₃H₆)2(C₂H₄)2N₄H₂(CH₂C₆H₅)2)(NO₃)]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

ammonium hexafluorophosphate + cadmium(II) nitrate tetrhydrate + 1,11-dibenzyl-1,4,8,11-tetraazacyclotetradecane (151367-38-3) → Cd(2+)*(C3H6)2(C2H4)2N4H2(CH2C6H5)2*NO3(1-)*PF6(1-)=[Cd((C3H6)2(C2H4)2N4H2(CH2C6H5)2)(NO3)]PF6 (578737-68-5)

Guidance literature:

In methanol; Cd-contg. compd. (0.105 mmol) in MeOH was added to a soln. of a ligand (0.105 mmol) in the same solvent; the soln. was stirred and heated for 0.5 h; the vol. of the soln. was reduced and excess satd. NH4PF6 in MeOH was added; the powder was filtered off and recrystd. from acetonitrile-isopropanol;elem. anal.;

DOI:10.1039/b300002h

upstream raw materials:

1,11-dibenzyl-1,4,8,11-tetraazacyclotetradecane

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