La₂(o-methylbenzoate)6(1,10-phenanthroline)2*H₂O

Base Information

• Chemical Name: La₂(o-methylbenzoate)6(1,10-phenanthroline)2*H₂O
• CAS No.: 1215781-47-7
• Molecular Formula: C₇₂H₅₈La₂N₄O₁₂*H₂O
• Molecular Weight: 1467.1
• Mol file: 1215781-47-7.mol

Synonyms:

Chemical Property of La₂(o-methylbenzoate)6(1,10-phenanthroline)2*H₂O

Chemical Property:

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Technology Process of La₂(o-methylbenzoate)6(1,10-phenanthroline)2*H₂O

There total 1 articles about La₂(o-methylbenzoate)6(1,10-phenanthroline)2*H₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ortho-methylbenzoic acid (118-90-1) + 1,10-Phenanthroline (66-71-7) + lanthanum(III) chloride hexahydrate (10025-84-0,20211-76-1) → La2(o-methylbenzoate)6(1,10-phenanthroline)2*H2O (1215781-47-7)

Guidance literature:

With aq.NaOH; In ethanol; water; o-methylbenzoic acid, 1,10-phenanthroline (3:1) dissolved in EtOH, pH adjusted to 6.0-7.0 (aq.NaOH), added dropwise toaq. soln. of LaCl3*6H2O (1equiv.), stirred for 5 h at room temp.; filtered, dried, elem. anal.;

DOI:10.1134/S1070328409070124

upstream raw materials:

ortho-methylbenzoic acid

1,10-Phenanthroline

lanthanum(III) chloride hexahydrate