(+/-)-cis-4-(dichloroacetyl-amino)-5-(4-nitro-phenyl)-dihydro-furan-2-one

Base Information

Chemical Name:(+/-)-cis-4-(dichloroacetyl-amino)-5-(4-nitro-phenyl)-dihydro-furan-2-one
CAS No.:100123-91-9
Molecular Formula:C₁₂H₁₀Cl₂N₂O₅
Molecular Weight:333.128
Hs Code.:

(+/-)-<i>cis</i>-4-(dichloroacetyl-amino)-5-(4-nitro-phenyl)-dihydro-furan-2-one

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-cis-4-(dichloroacetyl-amino)-5-(4-nitro-phenyl)-dihydro-furan-2-one

Chemical Property:

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Technology Process of (+/-)-cis-4-(dichloroacetyl-amino)-5-(4-nitro-phenyl)-dihydro-furan-2-one

There total 7 articles about (+/-)-cis-4-(dichloroacetyl-amino)-5-(4-nitro-phenyl)-dihydro-furan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99973-62-3
(+/-)-2r-(4-nitro-phenyl)-5-oxo-tetrahydro-furan-3t-carbonyl chloride

: 100123-91-9
(+/-)-trans-4-(dichloroacetyl-amino)-5-(4-nitro-phenyl)-dihydro-furan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: tetrachloromethane; aqueous sodium azide solution

2: dichloroacetic acid

With tetrachloromethane; dichloro-acetic acid; sodium azide;
DOI:10.1007/BF00902551

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 100123-91-9
(+/-)-trans-4-(dichloroacetyl-amino)-5-(4-nitro-phenyl)-dihydro-furan-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine

2: thionyl chloride

3: tetrachloromethane; aqueous sodium azide solution

4: dichloroacetic acid

With pyridine; tetrachloromethane; dichloro-acetic acid; thionyl chloride; sodium azide;
DOI:10.1007/BF00902551

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 100123-91-9
(+/-)-cis-4-(dichloroacetyl-amino)-5-(4-nitro-phenyl)-dihydro-furan-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine

2: thionyl chloride / Behandeln einer Loesung des Reaktionsprodukts in Tetrachlormethan mit wss. Natriumazid-Loesung

With pyridine; thionyl chloride;
DOI:10.1007/BF00902551