methyl (1RS,7RS,10RS,11RS)-2-(N-cyclohexylcarbamoyl)-4-methyl-3-oxo-6,6-diphenyl-2-azatetracyclo<5.3.1.0^1,5.0^10,11>undeca-4,8-diene-11-carboxylate

Base Information

• Chemical Name: methyl (1RS,7RS,10RS,11RS)-2-(N-cyclohexylcarbamoyl)-4-methyl-3-oxo-6,6-diphenyl-2-azatetracyclo<5.3.1.0^1,5.0^10,11>undeca-4,8-diene-11-carboxylate
• CAS No.: 136472-56-5
• Molecular Formula: C₃₂H₃₂N₂O₄
• Molecular Weight: 508.617

Synonyms:

Chemical Property of methyl (1RS,7RS,10RS,11RS)-2-(N-cyclohexylcarbamoyl)-4-methyl-3-oxo-6,6-diphenyl-2-azatetracyclo<5.3.1.0^1,5.0^10,11>undeca-4,8-diene-11-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of methyl (1RS,7RS,10RS,11RS)-2-(N-cyclohexylcarbamoyl)-4-methyl-3-oxo-6,6-diphenyl-2-azatetracyclo<5.3.1.0^1,5.0^10,11>undeca-4,8-diene-11-carboxylate

There total 3 articles about methyl (1RS,7RS,10RS,11RS)-2-(N-cyclohexylcarbamoyl)-4-methyl-3-oxo-6,6-diphenyl-2-azatetracyclo<5.3.1.0^1,5.0^10,11>undeca-4,8-diene-11-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

methyl (1RS,7SR)-2-(N-cyclohexylcarbamoyl)-4-methyl-3-oxo-6,6-diphenyl-2-azatricyclo<5.2.2.01,5>undeca-4,8,10-triene-8-carboxylate (136472-55-4) → methyl (1RS,7RS,10RS,11RS)-2-(N-cyclohexylcarbamoyl)-4-methyl-3-oxo-6,6-diphenyl-2-azatetracyclo<5.3.1.01,5.010,11>undeca-4,8-diene-11-carboxylate (136472-56-5)

Guidance literature:

In tetrahydrofuran; diethyl ether; for 2h; Irradiation;

DOI:10.1002/hlca.19910740512

Reference yield:

2-methyl-4,4-diphenylbuta-2,3-dienoic acid (6002-06-8) → methyl (1RS,7RS,10RS,11RS)-2-(N-cyclohexylcarbamoyl)-4-methyl-3-oxo-6,6-diphenyl-2-azatetracyclo<5.3.1.01,5.010,11>undeca-4,8-diene-11-carboxylate (136472-56-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 24 percent

2: 10 percent / diethyl ether; tetrahydrofuran / 2 h / Irradiation

In tetrahydrofuran; diethyl ether;

DOI:10.1002/hlca.19910740512

Reference yield:

3-Cyclohexyliminomethyleneamino-benzoic acid methyl ester → methyl (1RS,7RS,10RS,11RS)-2-(N-cyclohexylcarbamoyl)-4-methyl-3-oxo-6,6-diphenyl-2-azatetracyclo<5.3.1.01,5.010,11>undeca-4,8-diene-11-carboxylate (136472-56-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 24 percent

2: 10 percent / diethyl ether; tetrahydrofuran / 2 h / Irradiation

In tetrahydrofuran; diethyl ether;

DOI:10.1002/hlca.19910740512

upstream raw materials:

methyl (1RS,7SR)-2-(N-cyclohexylcarbamoyl)-4-methyl-3-oxo-6,6-diphenyl-2-azatricyclo<5.2.2.0^1,5>undeca-4,8,10-triene-8-carboxylate

2-methyl-4,4-diphenylbuta-2,3-dienoic acid

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