1H-Benzimidazole, 5,5'-methylenebis[2-[6-[1-[(3,5-dimethoxyphenyl)methyl]-1H-benzimidaz ol-2-yl]-2-pyridinyl]-1-methyl-

Base Information

Chemical Name:1H-Benzimidazole, 5,5'-methylenebis[2-[6-[1-[(3,5-dimethoxyphenyl)methyl]-1H-benzimidaz ol-2-yl]-2-pyridinyl]-1-methyl-
CAS No.:144493-37-8
Molecular Formula:C₅₉H₅₀N₁₀O₄
Molecular Weight:963.111
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-Benzimidazole, 5,5'-methylenebis[2-[6-[1-[(3,5-dimethoxyphenyl)methyl]-1H-benzimidaz ol-2-yl]-2-pyridinyl]-1-methyl-

Chemical Property:

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Technology Process of 1H-Benzimidazole, 5,5'-methylenebis[2-[6-[1-[(3,5-dimethoxyphenyl)methyl]-1H-benzimidaz ol-2-yl]-2-pyridinyl]-1-methyl-

There total 1 articles about 1H-Benzimidazole, 5,5'-methylenebis[2-[6-[1-[(3,5-dimethoxyphenyl)methyl]-1H-benzimidaz ol-2-yl]-2-pyridinyl]-1-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 877-88-3
3,5-dimethoxybenzyl bromide

: 150022-60-9
bis<1-methyl-2-(6'-pyrid-2'-yl)benzimidazol-5-yl>methane

: 144493-37-8
bis<1-methyl-2-(6'-<1-(3,5-dimethoxybenzyl)benzimidazol-2-yl>pyrid-2'-yl)benzimidazol-5-yl>methane

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMF, RT, 1 h, 2.) DMF, 15 h;
DOI:10.1021/ja00071a032

Reference yield: 80.0%

: europium(III) perchlorate hydrate

: 144493-37-8
bis<1-methyl-2-(6'-<1-(3,5-dimethoxybenzyl)benzimidazol-2-yl>pyrid-2'-yl)benzimidazol-5-yl>methane

: {Eu₂(bis(1-methyl-2-(6-{1-(3,5-dimethoxybenzyl)benzimidazol-2-yl}pyrid-2-yl)benzimidazol-5-yl)methane)3}(ClO₄)6 * 9 acetonitrile

Guidance literature:: In acetonitrile; diffusion of gaseous diethyl ether into the concd. soln., pptd.;

Reference yield:

: lanthanum(III) perchlorate hydrate

: 144493-37-8
bis<1-methyl-2-(6'-<1-(3,5-dimethoxybenzyl)benzimidazol-2-yl>pyrid-2'-yl)benzimidazol-5-yl>methane

: 2La⁽³⁺⁾*3((C₆H₃(OCH₃)2CH₂C₇H₄N₂C₅H₃NC₇H₃N₂(CH₃))2CH₂)*6ClO₄^(1-)*2H₂O*CH₃CN={La₂(C₅₉H₅₀N₁₀O₄)3}(ClO₄)6*2H₂O*CH₃CN

Guidance literature:: In dichloromethane; acetonitrile; a soln. of La(ClO4)3*99H2O added slowly to a soln. of N-compound in acetonitrile/dichloromethane; evapd.; dissolved in acetonitrile; diethyl ether allowed to diffuse into the soln. for 3 days; filtered; yield: 70-90%; elem. anal.;
DOI:10.1021/ja00071a032