Technology Process of 1H-Indole-4,5-dicarboxylic acid, 6-hydroxy-1-(phenylmethyl)-, dimethyl
ester
There total 3 articles about 1H-Indole-4,5-dicarboxylic acid, 6-hydroxy-1-(phenylmethyl)-, dimethyl
ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 75 percent / 50percent NaOH, triethylbenzylammonium bromide / benzene / 4 h / 60 °C
2: 86 percent / 5percent NaOH / ethanol / 2 h / Heating
3: 61 percent / copper chromite, quinoline / 4 h / 150 °C
4: 50 percent / acetonitrile
With
quinoline; sodium hydroxide; copper chromite; benzyltriethylammonium bromide;
In
ethanol; acetonitrile; benzene;
DOI:10.1135/cccc19921487
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 86 percent / 5percent NaOH / ethanol / 2 h / Heating
2: 61 percent / copper chromite, quinoline / 4 h / 150 °C
3: 50 percent / acetonitrile
With
quinoline; sodium hydroxide; copper chromite;
In
ethanol; acetonitrile;
DOI:10.1135/cccc19921487
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 61 percent / copper chromite, quinoline / 4 h / 150 °C
2: 50 percent / acetonitrile
With
quinoline; copper chromite;
In
acetonitrile;
DOI:10.1135/cccc19921487