N,N-Dimethyl-1-(2,4-cyclopentenylidene)ethanamine

Base Information

Chemical Name:N,N-Dimethyl-1-(2,4-cyclopentenylidene)ethanamine
CAS No.:14469-77-3
Molecular Formula:C9H13N
Molecular Weight:135.209
Hs Code.:
Mol file:14469-77-3.mol

Synonyms:6-(Dimethylamino)-6-methylfulvene;6-methyl-6-dimethylaminofulvene;6-methyl-6-(dimethylamino)pentafulvene;6-N,N-dimethylamino-6-methylfulvene;6-dimethylamino-6-methylfulvene;6-methyl-6-N,N-dimethylaminofulvene;

Suppliers and Price of N,N-Dimethyl-1-(2,4-cyclopentenylidene)ethanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N,N-Dimethyl-1-(2,4-cyclopentenylidene)ethanamine

Chemical Property:

PSA：3.24000
LogP:1.94800

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N,N-Dimethyl-1-(2,4-cyclopentenylidene)ethanamine

There total 7 articles about N,N-Dimethyl-1-(2,4-cyclopentenylidene)ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 18871-66-4
N,N-dimethylacetamide dimethyl acetal

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 14469-77-3
6-methyl-6-dimethylaminofulvene

Guidance literature:: at 20 ℃; for 22h;
DOI:10.3987/COM-05-10535

Reference yield: 66.7%

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 19429-85-7
N,N-dimethylacetamide diethyl acetal

: 14469-77-3
6-methyl-6-dimethylaminofulvene

Guidance literature:: for 18h; Ambient temperature;
DOI:10.1021/jo00339a043

Reference yield:

: 127-19-5,116057-81-9
N,N-dimethyl acetamide

: sodium cyclopentadienide

: 14469-77-3
6-methyl-6-dimethylaminofulvene

Guidance literature:: With dimethyl sulfate; Yield given. Multistep reaction; 1.) 70 deg C to 80 deg C, 2 h; 2.) THF, -10 deg C to -5 deg C;
DOI:10.1002/(SICI)1099-0682(199808)1998:8<1153::AID-EJIC1153>3.0.CO;2-R