4-Chloro-3-nitrobenzene-1,2-diamine

Base Information

Chemical Name:4-Chloro-3-nitrobenzene-1,2-diamine
CAS No.:144729-44-2
Molecular Formula:C6H6ClN3O2
Molecular Weight:187.586
Hs Code.:
DSSTox Substance ID:DTXSID40395745
Nikkaji Number:J2.193.096B
Wikidata:Q82195991
Mol file:144729-44-2.mol

Synonyms:4-chloro-3-nitrobenzene-1,2-diamine;144729-44-2;1,2-Benzenediamine, 4-chloro-3-nitro-;4-chloro-3-nitro-1,2-benzenediamine;4-chloro-3-nitro-1,2-phenylenediamine;SCHEMBL1030166;DTXSID40395745;OHIUWWQDSMTIFW-UHFFFAOYSA-N;MFCD02169899;3-Nitro-4-chloro-1,2-benzenediamine;AKOS015994233;MS-2335;4-chloro-3-nitro-benzene-1,2-diamine;CS-0186987;E74344

Suppliers and Price of 4-Chloro-3-nitrobenzene-1,2-diamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 4-Chloro-3-nitrobenzene-1,2-diamine

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:187.0148541
Heavy Atom Count:12
Complexity:184

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C(=C1N)N)[N+](=O)[O-])Cl

Technology Process of 4-Chloro-3-nitrobenzene-1,2-diamine

There total 5 articles about 4-Chloro-3-nitrobenzene-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 20718-46-1
5-chloro-4-nitro-2,1,3-benzoselenadiazole

: 144729-44-2
4-chloro-3-nitro-1,2-phenylenediamine

Guidance literature:: With hydrogenchloride; hydrogen iodide; In water; at 20 ℃; for 2h;
DOI:10.1016/j.tetlet.2005.04.145

Reference yield:

: 95-83-0
4-Chloro-1,2-phenylenediamine

: 144729-44-2
4-chloro-3-nitro-1,2-phenylenediamine

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / SeO₂

2: 90 percent / NaNO₃; aq. H₂SO₄ / 100 °C

3: 52 percent / aq. HI; aq. HCl

With hydrogenchloride; sodium nitrate; selenium(IV) oxide; sulfuric acid; hydrogen iodide;
DOI:10.1023/B:RUGC.0000030402.66220.55

Reference yield:

: 1123-92-8,6343-86-8
5-chloro-benzo[1,2,5]selenadiazole

: 144729-44-2
4-chloro-3-nitro-1,2-phenylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / NaNO₃; aq. H₂SO₄ / 100 °C

2: 52 percent / aq. HI; aq. HCl

With hydrogenchloride; sodium nitrate; sulfuric acid; hydrogen iodide;
DOI:10.1023/B:RUGC.0000030402.66220.55