1(2H)-Pyridinecarboxylic acid, 3,4-dihydro-4-hydroxy-2-(triphenylsilyl)-, (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester, (2S,4R)-

Base Information

Chemical Name:1(2H)-Pyridinecarboxylic acid, 3,4-dihydro-4-hydroxy-2-(triphenylsilyl)-, (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester, (2S,4R)-
CAS No.:145238-77-3
Molecular Formula:C40H45NO3Si
Molecular Weight:615.888
Hs Code.:
Mol file:145238-77-3.mol

1(2H)-Pyridinecarboxylic acid, 3,4-dihydro-4-hydroxy-2-(triphenylsilyl)-,
(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester,
(2S,4R)-

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1(2H)-Pyridinecarboxylic acid, 3,4-dihydro-4-hydroxy-2-(triphenylsilyl)-, (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester, (2S,4R)-

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Technology Process of 1(2H)-Pyridinecarboxylic acid, 3,4-dihydro-4-hydroxy-2-(triphenylsilyl)-, (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester, (2S,4R)-

There total 5 articles about 1(2H)-Pyridinecarboxylic acid, 3,4-dihydro-4-hydroxy-2-(triphenylsilyl)-, (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester, (2S,4R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 131426-68-1
(-)-1-((1R,2S,5R)-8-phenylmenthoxycarbonyl)-(S)-2-triphenylsilyl-2,3-dihydro-4-pyridone

: 145238-77-3
(R)-4-hydroxy-1-((1R,2S,5R)-8-phenylmenthoxycarbonyl)-(S)-2-triphenylsilyl-1,2,3,4-tetrahydropyridine

Guidance literature:: With sodium tetrahydroborate; cerium(III) chloride; In methanol;
DOI:10.1021/ja00053a050

Reference yield:

: 126378-43-6
(1R,2S,5R)-(-)-8-phenylmenthyl chloroformate

: 145238-77-3
(R)-4-hydroxy-1-((1R,2S,5R)-8-phenylmenthoxycarbonyl)-(S)-2-triphenylsilyl-1,2,3,4-tetrahydropyridine

Guidance literature:: Multi-step reaction with 2 steps

2: 98 percent / NaBH₄, CeCl₃ / methanol

With sodium tetrahydroborate; cerium(III) chloride; In methanol;
DOI:10.1021/ja00053a050

Reference yield:

: 620-08-6,1232006-56-2
4-methoxypyridine

: 145238-77-3
(R)-4-hydroxy-1-((1R,2S,5R)-8-phenylmenthoxycarbonyl)-(S)-2-triphenylsilyl-1,2,3,4-tetrahydropyridine

Guidance literature:: Multi-step reaction with 2 steps

2: 98 percent / NaBH₄, CeCl₃ / methanol

With sodium tetrahydroborate; cerium(III) chloride; In methanol;
DOI:10.1021/ja00053a050