BOC-L-ISOLEUCINE THIOAMIDE

Base Information

Chemical Name:BOC-L-ISOLEUCINE THIOAMIDE
CAS No.:145491-31-2
Molecular Formula:C11H22N2O2S
Molecular Weight:246.37000
Hs Code.:
Mol file:145491-31-2.mol

Synonyms:Boc-isoleucine thioamide;Boc-His(Dnp)-OH;Nalpha-Boc-N(im)-2,4-dinitrophenyl-L-histidine;

Suppliers and Price of BOC-L-ISOLEUCINE THIOAMIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
BOC-L-ISOLEUCINE THIOAMIDE 95.00%
5MG
$ 498.40

Total 1 raw suppliers

Chemical Property of BOC-L-ISOLEUCINE THIOAMIDE

Chemical Property:

PSA：104.47000
LogP:3.13700

Purity/Quality:: BOC-L-ISOLEUCINE THIOAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of BOC-L-ISOLEUCINE THIOAMIDE

There total 4 articles about BOC-L-ISOLEUCINE THIOAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 94888-34-3
tert-butyl ((2S,3S)-1-amino-3-methyl-1-oxopentan-2-yl)carbamate

: 145491-31-2
Boc-isoleucine thioamide

Guidance literature:: With 2,4-(4-phenoxyphenyl)-1,3-dithia-2λ(5),4λ(5)-diphosphetane 2,4-disulfides; In tetrahydrofuran; for 6h; Ambient temperature;
DOI:10.1021/jo00215a040

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 145491-31-2
Boc-isoleucine thioamide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / triethylamine / CH₂Cl₂ / 3 h

2: 86 percent / 2,4-bis(4-phenoxyphenyl)-1,3-dithia-2,4-diphosphetane 2,4-disulfide (PTPS) / tetrahydrofuran / 6 h / Ambient temperature

With 2,4-(4-phenoxyphenyl)-1,3-dithia-2λ(5),4λ(5)-diphosphetane 2,4-disulfides; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00215a040

Reference yield:

: 10466-56-5
L-isoleucine amide hydrochloride

: 145491-31-2
Boc-isoleucine thioamide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / triethylamine / CH₂Cl₂ / 3 h

2: 86 percent / 2,4-bis(4-phenoxyphenyl)-1,3-dithia-2,4-diphosphetane 2,4-disulfide (PTPS) / tetrahydrofuran / 6 h / Ambient temperature

With 2,4-(4-phenoxyphenyl)-1,3-dithia-2λ(5),4λ(5)-diphosphetane 2,4-disulfides; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00215a040