[PuO₂(1,10-phenanthroline)(benzoate)] [PuO₂(C₁₂N₂H₈)(OOCC₆H₅)], high temperature

Base Information

• Chemical Name: [PuO₂(1,10-phenanthroline)(benzoate)] [PuO₂(C₁₂N₂H₈)(OOCC₆H₅)], high temperature
• CAS No.: 1214279-27-2
• Molecular Formula: C₇H₅O₂*C₁₂H₈N₂*O₂Pu
• Molecular Weight: 577.387

Synonyms:

Chemical Property of [PuO₂(1,10-phenanthroline)(benzoate)] [PuO₂(C₁₂N₂H₈)(OOCC₆H₅)], high temperature

Chemical Property:

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Technology Process of [PuO₂(1,10-phenanthroline)(benzoate)] [PuO₂(C₁₂N₂H₈)(OOCC₆H₅)], high temperature

There total 2 articles about [PuO₂(1,10-phenanthroline)(benzoate)] [PuO₂(C₁₂N₂H₈)(OOCC₆H₅)], high temperature which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,10-Phenanthroline (66-71-7) + plutonyl(VI) perchlorate + ammonium benzoate (1863-63-4) → [PuO2(1,10-phenanthroline)(benzoate)] [PuO2(C12N2H8)(OOCC6H5)], low temperature (1214279-27-2)

Guidance literature:

In water; soln. of PuO2(ClO4)2 diluted with water and soln. of ammonium benzoate and N2H4 added; resulting soln. mixed and then phen soln. added; ppt. formed for 1-2 d at room temp.; ppt. filtered off in vac. on glass frit, washed with water, dried in airflow; TGA;

DOI:10.1134/S1066362209030035

Reference yield:

1,10-Phenanthroline (66-71-7) + plutonyl(VI) perchlorate + ammonium benzoate (1863-63-4) → [PuO2(1,10-phenanthroline)(benzoate)] [PuO2(C12N2H8)(OOCC6H5)], high temperature (1214279-27-2)

Guidance literature:

In water; soln. of PuO2(ClO4)2 diluted with water and soln. of ammonium benzoate and N2H4 added; resulting soln. mixed and then phen soln. added; ppt. formed for 7-9 h on heating to 65-70°C; ppt. filtered off in vac. on glass frit, washed with water, dried in airflow; TGA;

DOI:10.1134/S1066362209030035

upstream raw materials:

1,10-Phenanthroline

ammonium benzoate

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