Phosphinecarbothioamide, 1,1-dicyclohexyl-N-phenyl-, 1-sulfide

Base Information

• Chemical Name: Phosphinecarbothioamide, 1,1-dicyclohexyl-N-phenyl-, 1-sulfide
• CAS No.: 14633-83-1
• Molecular Formula: C₁₉H₂₈NPS₂
• Molecular Weight: 365.544
• Mol file: 14633-83-1.mol

Synonyms:

Chemical Property of Phosphinecarbothioamide, 1,1-dicyclohexyl-N-phenyl-, 1-sulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Phosphinecarbothioamide, 1,1-dicyclohexyl-N-phenyl-, 1-sulfide

There total 1 articles about Phosphinecarbothioamide, 1,1-dicyclohexyl-N-phenyl-, 1-sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ Dicyclohexyl--phosphinsulfid (14633-83-1)

Guidance literature:

Dicyclohexyl--phosphin, Schwefel in sd. A.;

DOI:10.1002/zaac.19673510104

Reference yield:

ethylenebis(triphenylphosphine)platinum(0) (12120-15-9) + Dicyclohexyl--phosphinsulfid (14633-83-1) → ((C6H5)3P)2Pt((C6H11)2P(S)C(S)NHC6H5)

Guidance literature:

In benzene; equimolar amts. (PPh3)2PtC2H4 and Cy2P(S)C(S)NPhH stirred in benzene at0°C for 10 min under N2 atm.; hexane added; elem. anal.;

Reference yield:

copper(ll) sulfate pentahydrate + Dicyclohexyl--phosphinsulfid (14633-83-1) → bis[N-phenyl(dicyclohexylthiophosphinoyl)thiomethanamido-S,S']copper(II) (316373-45-2)

Guidance literature:

In ethanol; dichloromethane; CuSO4*5H2O and a twofold molar excess of Cy2PSCSNHPh in ethanol/CH2Cl2 (1/1); ppt., recrystd. from CH2Cl2 by slow evapn. of the solvent at 295 K;

DOI:10.1107/S0108270100011586

Downstream raw materials:

bis[N-phenyl(dicyclohexylthiophosphinoyl)thiomethanamido-S,S']copper(II)