Prop-2-en-1-yl phenyl(prop-2-en-1-yl)phosphinate

Base Information

Chemical Name:Prop-2-en-1-yl phenyl(prop-2-en-1-yl)phosphinate
CAS No.:14655-46-0
Molecular Formula:C12H15O2P
Molecular Weight:222.224
Hs Code.:
DSSTox Substance ID:DTXSID90544185
Nikkaji Number:J1.290.294H
Mol file:14655-46-0.mol

Synonyms:14655-46-0;Prop-2-en-1-yl phenyl(prop-2-en-1-yl)phosphinate;SCHEMBL11319680;DTXSID90544185

Suppliers and Price of Prop-2-en-1-yl phenyl(prop-2-en-1-yl)phosphinate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Prop-2-en-1-yl phenyl(prop-2-en-1-yl)phosphinate

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:222.08096671
Heavy Atom Count:15
Complexity:254

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCOP(=O)(CC=C)C1=CC=CC=C1

Technology Process of Prop-2-en-1-yl phenyl(prop-2-en-1-yl)phosphinate

There total 5 articles about Prop-2-en-1-yl phenyl(prop-2-en-1-yl)phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 833-57-8
bis-(allyloxy)phenylphosphane

: 14655-46-0
allylphenylphosphinic acid allyl ester

Guidance literature:: With trimethylsilyl bromide; at 80 ℃; Inert atmosphere;
DOI:10.1002/chem.200800435

Reference yield:

: 833-57-8
bis-(allyloxy)phenylphosphane

: 14655-46-0
allylphenylphosphinic acid allyl ester

: 2948-89-2
phenylphosphonic acid diallyl ester

Guidance literature:: at 130 ℃;
DOI:10.1016/S0040-4020(00)00080-6

Reference yield:

: 644-97-3
Dichlorophenylphosphine

: 14655-46-0
allylphenylphosphinic acid allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / diethyl ether / 0 - 20 °C / Heating

2: 0.5 g / 130 °C

With pyridine; In diethyl ether; 1: Substitution / 2: Rearrangement;
DOI:10.1016/S0040-4020(00)00080-6