Bicyclo[3.2.0]hept-3-en-6-one, 1,4-dimethyl-

Base Information

Chemical Name:Bicyclo[3.2.0]hept-3-en-6-one, 1,4-dimethyl-
CAS No.:146607-24-1
Molecular Formula:C9H12O
Molecular Weight:136.19100
Hs Code.:
DSSTox Substance ID:DTXSID90436834
Mol file:146607-24-1.mol

Synonyms:Bicyclo[3.2.0]hept-3-en-6-one, 1,4-dimethyl-;146607-24-1;SCHEMBL9246486;DTXSID90436834;4-BROMO-4-(4-CHLOROPHENYL)PIPERIDINE HYDROBROMIDE

Suppliers and Price of Bicyclo[3.2.0]hept-3-en-6-one, 1,4-dimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bicyclo[3.2.0]hept-3-en-6-one, 1,4-dimethyl-

Chemical Property:

PSA：17.07000
LogP:1.93170
XLogP3:1.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:136.088815002
Heavy Atom Count:10
Complexity:227

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CCC2(C1C(=O)C2)C

Technology Process of Bicyclo[3.2.0]hept-3-en-6-one, 1,4-dimethyl-

There total 4 articles about Bicyclo[3.2.0]hept-3-en-6-one, 1,4-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3240-09-3
5-methyl-5-hexen-2-one

: 146607-24-1,133700-21-7
1,4-dimethylbicyclo<3.2.0>hept-3-en-6-one

Guidance literature:: Multi-step reaction with 2 steps

1: 1) hexamethyldisilazane, n-BuLi / 1) THF, -60 deg C, 1.5h, 2) to r.t., overnight

With n-butyllithium; 1,1,1,3,3,3-hexamethyl-disilazane;
DOI:10.1021/jo00010a033

Reference yield:

: 73516-48-0
Ethyl (E)-3,6-dimethyl-2,6-heptadienoate

: 146607-24-1,133700-21-7
1,4-dimethylbicyclo<3.2.0>hept-3-en-6-one

: 104923-42-4
1-methyl-4-methylenebicyclo<3.2.0>heptan-6-one

Guidance literature:: With methanol; potassium hydroxide; sodium acetate; acetic anhydride; Yield given. Multistep reaction. Yields of byproduct given; 1) reflux, 4h, 2) reflux, 4h;
DOI:10.1021/jo00010a033