trans-5-methyl-2-phenyl-4-vinyl-1,2-oxaborolane

Base Information

Chemical Name:trans-5-methyl-2-phenyl-4-vinyl-1,2-oxaborolane
CAS No.:143447-14-7
Molecular Formula:C₁₂H₁₅BO
Molecular Weight:186.062
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-5-methyl-2-phenyl-4-vinyl-1,2-oxaborolane

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Technology Process of trans-5-methyl-2-phenyl-4-vinyl-1,2-oxaborolane

There total 1 articles about trans-5-methyl-2-phenyl-4-vinyl-1,2-oxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84017-49-2
1-phenyl-2,5-dihydro-1H-borole

: 75-07-0,9002-91-9
acetaldehyde

: 143447-14-7
trans-5-methyl-2-phenyl-4-vinyl-1,2-oxaborolane

: 143446-94-0
cis-5-methyl-2-phenyl-4-vinyl-1,2-oxaborolane

Guidance literature:: In diethyl ether; dropping aldehyde to soln. of 3-borolene in diethyl ether at -78°C, stirring, under N2; slow warming to room temp.; mechanism discussed;; product mixt. cis/trans=97:3 with 94 % yield obtained; removal of solvent in vac.; distn. in vac.; elem. anal.; b. p.; NMR spectroscopy;;