<9-Phenyl-fluorenyl-(9)>-carbonyldiazomethan

Base Information Edit

Chemical Name:<9-Phenyl-fluorenyl-(9)>-carbonyldiazomethan
CAS No.:18554-45-5
Molecular Formula:C₂₁H₁₄N₂O
Molecular Weight:310.355
Hs Code.:
Mol file:18554-45-5.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <9-Phenyl-fluorenyl-(9)>-carbonyldiazomethan Edit

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Technology Process of <9-Phenyl-fluorenyl-(9)>-carbonyldiazomethan

There total 1 articles about <9-Phenyl-fluorenyl-(9)>-carbonyldiazomethan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 18554-43-3
9-carboxy-9-phenylfluorene

: 18554-45-5
<9-Phenyl-fluorenyl-(9)>-carbonyldiazomethan

Guidance literature:: Multistep reaction; (i) SOCl₂, (ii) /BRN= 102415/;
DOI:10.1021/jo01260a032

Reference yield:

: 18554-45-5
<9-Phenyl-fluorenyl-(9)>-carbonyldiazomethan

: <9-Phenyl-fluorenyl-(9)>-essigsaeure-n-hexylester

Guidance literature:: Multi-step reaction with 2 steps

1: (i) 4-ethyl-morpholine, hexan-1-ol (heating), (ii) KOH

2: H₂SO₄

With sulfuric acid;
DOI:10.1021/jo01260a032