2-(2-THIENYLMETHYL)BENZOIC ACID

Base Information

Chemical Name:2-(2-THIENYLMETHYL)BENZOIC ACID
CAS No.:62636-87-7
Molecular Formula:C12H10 O2 S
Molecular Weight:218.276
Hs Code.:2934999090
Mol file:62636-87-7.mol

Synonyms:o-Toluicacid, a-2-thienyl- (7CI);2-(Thiophen-2-ylmethyl)benzoic acid; NSC 241141

Suppliers and Price of 2-(2-THIENYLMETHYL)BENZOIC ACID

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
2-Thiophen-2-ylmethyl-benzoic acid
1g
$ 378.00

Crysdot
2-(Thiophen-2-ylmethyl)benzoicacid 97%
5g
$ 874.00

Arctom
2-(Thiophen-2-ylmethyl)benzoicacid
1g
$ 291.00

American Custom Chemicals Corporation
2-THIOPHEN-2-YLMETHYL-BENZOIC ACID 95.00%
500MG
$ 796.95

AK Scientific
2-Thiophen-2-ylmethyl-benzoicacid
1g
$ 560.00

Total 10 raw suppliers

Chemical Property of 2-(2-THIENYLMETHYL)BENZOIC ACID

Chemical Property:

Vapor Pressure:4.39E-06mmHg at 25°C
Boiling Point:368.6°C at 760 mmHg
Flash Point:176.7°C
PSA：65.54000
Density:1.277g/cm³
LogP:3.03710

Purity/Quality:

97% ^*data from raw suppliers

2-Thiophen-2-ylmethyl-benzoic acid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(2-THIENYLMETHYL)BENZOIC ACID

There total 5 articles about 2-(2-THIENYLMETHYL)BENZOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 46496-80-4
2-(thiophene-2-carbonyl)-benzoic acid

: 62636-87-7
2-(thiophene-2-yl-methyl)-benzoic acid

Guidance literature:: With ammonium hydroxide; zinc; Heating;

Reference yield: 75.0%

: 147437-99-8
3-(thiophen-2-yl)isobenzofuran-1(3H)-one

: 62636-87-7
2-(thiophene-2-yl-methyl)-benzoic acid

Guidance literature:: With palladium on activated carbon; hydrogen; acetic acid; at 90 ℃; for 4h; under 760.051 Torr; Schlenk technique;
DOI:10.1021/acs.orglett.9b02673

Reference yield:

: 85-44-9
phthalic anhydride

: 62636-87-7
2-(thiophene-2-yl-methyl)-benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: AlCl₃ / CH₂Cl₂ / 0.5 h / 20 °C

1.2: 70 percent / CH₂Cl₂ / 3 h / 20 °C

2.1: 60 percent / aq. NH₃; CuSO₄; Zn / 48 h / Heating

With ammonium hydroxide; aluminium trichloride; copper(II) sulfate; zinc; In dichloromethane; 1.2: Friedel-Crafts acylation;
DOI:10.1021/jm0605031