N-[2-(Benzenesulfinyl)ethyl]-N-[(3,4-dimethoxyphenyl)methyl]acetamide

Base Information

Chemical Name:N-[2-(Benzenesulfinyl)ethyl]-N-[(3,4-dimethoxyphenyl)methyl]acetamide
CAS No.:148679-46-3
Molecular Formula:C19H23NO4S
Molecular Weight:361.462
Hs Code.:
DSSTox Substance ID:DTXSID90571552
Mol file:148679-46-3.mol

Synonyms:148679-46-3;N-[2-(Benzenesulfinyl)ethyl]-N-[(3,4-dimethoxyphenyl)methyl]acetamide;DTXSID90571552

Suppliers and Price of N-[2-(Benzenesulfinyl)ethyl]-N-[(3,4-dimethoxyphenyl)methyl]acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-[2-(Benzenesulfinyl)ethyl]-N-[(3,4-dimethoxyphenyl)methyl]acetamide

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:8
Exact Mass:361.13477939
Heavy Atom Count:25
Complexity:439

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)N(CCS(=O)C1=CC=CC=C1)CC2=CC(=C(C=C2)OC)OC

Technology Process of N-[2-(Benzenesulfinyl)ethyl]-N-[(3,4-dimethoxyphenyl)methyl]acetamide

There total 8 articles about N-[2-(Benzenesulfinyl)ethyl]-N-[(3,4-dimethoxyphenyl)methyl]acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 148679-80-5
N-acetyl-N-(3,4-dimethoxyphenyl)methyl-2-(phenylthio)ethylamine

: 148679-46-3
N-acetyl-N-(3,4-dimethoxyphenyl)methyl-2-(phenylsulfinyl)ethylamine

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -30 ℃; for 2.5h;
DOI:10.3987/COM-92-S14

Reference yield:

: 148679-35-0
N-(3,4-dimethoxyphenyl)methyl-2-(phenylthio)ethylamine

: 148679-46-3
N-acetyl-N-(3,4-dimethoxyphenyl)methyl-2-(phenylsulfinyl)ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / pyridine / 16 h / Ambient temperature

2: 93 percent / aq. NaIO₄ / methanol / 20 h / Ambient temperature

With pyridine; sodium periodate; In methanol;
DOI:10.1248/cpb.45.813

Reference yield:

: 2014-75-7
2-(phenylthio)ethanamine

: 148679-46-3
N-acetyl-N-(3,4-dimethoxyphenyl)methyl-2-(phenylsulfinyl)ethylamine

Guidance literature:: Multi-step reaction with 4 steps

1: AcOH / ethanol / 20 h / Heating

2: NaBH₄ / methanol / 1 h / Ambient temperature

3: 96 percent / pyridine / 16 h / Ambient temperature

4: 93 percent / aq. NaIO₄ / methanol / 20 h / Ambient temperature

With pyridine; sodium tetrahydroborate; sodium periodate; acetic acid; In methanol; ethanol;
DOI:10.1248/cpb.45.813