(2,6-diisopropylphenylimido)bis(1,1-dimethyl-2,2,2-trifluoroethanolato)(triphenylvinylstannane)molybdenium(IV)

Base Information

• Chemical Name: (2,6-diisopropylphenylimido)bis(1,1-dimethyl-2,2,2-trifluoroethanolato)(triphenylvinylstannane)molybdenium(IV)
• CAS No.: 1361015-86-2
• Molecular Formula: C₄₀H₄₇F₆MoNO₂Sn
• Molecular Weight: 902.459
• Mol file: 1361015-86-2.mol

Synonyms:

Chemical Property of (2,6-diisopropylphenylimido)bis(1,1-dimethyl-2,2,2-trifluoroethanolato)(triphenylvinylstannane)molybdenium(IV)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2,6-diisopropylphenylimido)bis(1,1-dimethyl-2,2,2-trifluoroethanolato)(triphenylvinylstannane)molybdenium(IV)

There total 1 articles about (2,6-diisopropylphenylimido)bis(1,1-dimethyl-2,2,2-trifluoroethanolato)(triphenylvinylstannane)molybdenium(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

{(2-methyl-2-phenyl-propylidene)((2,6-diisopropylphenyl)imido)molybdenum(VI)bis(trifluoro-tert-butoxide)} (149883-24-9,149883-25-0,135505-85-0) + triphenyl-vinyl stannane (2117-48-8) → 2-methyl-2-phenyl-5-(triphenylstannyl)pent-3-ene (1361015-92-0) + (2,6-diisopropylphenylimido)bis(1,1-dimethyl-2,2,2-trifluoroethanolato)(triphenylvinylstannane)molybdenium(IV) (1361015-86-2)

Guidance literature:

In benzene-d6; using Schlenk techniques; to soln. of Mo complex in C6D6 was added soln.of Ph3SnCHCH2 in C6D6 at room temp.; monitored by NMR spectroscopy; after 10 min solvent removed by evapn. (vac.);

DOI:10.1134/S1070363212010033

upstream raw materials:

{(2-methyl-2-phenyl-propylidene)((2,6-diisopropylphenyl)imido)molybdenum(VI)bis(trifluoro-tert-butoxide)}

triphenyl-vinyl stannane